Journal of Thermal Analysis and Calorimetry
Volume/Issue:
Volume 96: Issue 2
Isoconversional kinetic analysis of resol-clay nanocomposites
Authors:
M. López Universidad País Vasco/Euskal Herriko Unibertsitatea Materials and Technologies’ Group, Escuela Politécnica, Department of Chemical & Environmental Engineering Pza. Europa 1 20018 Donostia-San Sebastián Spain

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M. Blanco Universidad País Vasco/Euskal Herriko Unibertsitatea Materials and Technologies’ Group, Escuela Politécnica, Department of Chemical & Environmental Engineering Pza. Europa 1 20018 Donostia-San Sebastián Spain

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A. Vazquez Universidad País Vasco/Euskal Herriko Unibertsitatea Materials and Technologies’ Group, Escuela Politécnica, Department of Chemical & Environmental Engineering Pza. Europa 1 20018 Donostia-San Sebastián Spain

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J. Ramos Universidad País Vasco/Euskal Herriko Unibertsitatea Materials and Technologies’ Group, Escuela Politécnica, Department of Chemical & Environmental Engineering Pza. Europa 1 20018 Donostia-San Sebastián Spain

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A. Arbelaiz Universidad País Vasco/Euskal Herriko Unibertsitatea Materials and Technologies’ Group, Escuela Politécnica, Department of Chemical & Environmental Engineering Pza. Europa 1 20018 Donostia-San Sebastián Spain

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N. Gabilondo Universidad País Vasco/Euskal Herriko Unibertsitatea Materials and Technologies’ Group, Escuela Politécnica, Department of Chemical & Environmental Engineering Pza. Europa 1 20018 Donostia-San Sebastián Spain

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J. Echeverría Hexion Specialty Chemicals Ibérica Ctra. Navarra Epele 39 20120 Hernani (Gipuzkoa) Spain

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I. Mondragon Universidad País Vasco/Euskal Herriko Unibertsitatea Materials and Technologies’ Group, Escuela Politécnica, Department of Chemical & Environmental Engineering Pza. Europa 1 20018 Donostia-San Sebastián Spain

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Pages:
567–573
Online Publication Date:
13 Nov 2008
Publication Date:
01 May 2009
Article Category:
Research Article
DOI:
https://doi.org/10.1007/s10973-008-9212-y
Keywords:
curing; kinetics; montmorillonite; nanocomposites; resols
Restricted access

Abstract  

The curing kinetics of nanocomposites based on phenolic resol cured with triethylamine (TEA) containing different amounts of organic montmorillonite was analyzed by differential scanning calorimetry. Kissinger-Akahira-Sunose (KAS) model-free kinetics has been applied to correlate the dynamic cure behaviour in the presence of modified montmorillonite. The effect in the curing of the use of different clay modifiers has also been studied. A commercial clay with hydroxyl groups (Cloisite 30B) and a customized montmorillonite (PheMMT) whose reactive groups induce condensation reactions with the resol matrix have been used. Strong dependency of activation energy on apparent conversion has been observed for all compounds.

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Cover Journal of Thermal Analysis and Calorimetry
Journal of Thermal Analysis and Calorimetry
Print ISSN:
1388-6150
Online ISSN:
1572-8943

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Journal of Thermal Analysis and Calorimetry
Language English
Size A4
Year of
Foundation		 1969
Volumes
per Year		 1
Issues
per Year		 24
Founder Akadémiai Kiadó
Founder's
Address		 H-1117 Budapest, Hungary 1516 Budapest, PO Box 245.
Publisher Akadémiai Kiadó
Springer Nature Switzerland AG
Publisher's
Address		 H-1117 Budapest, Hungary 1516 Budapest, PO Box 245.
CH-6330 Cham, Switzerland Gewerbestrasse 11.
Responsible
Publisher		 Chief Executive Officer, Akadémiai Kiadó
ISSN 1388-6150 (Print)
ISSN 1588-2926 (Online)

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