Journal of Thermal Analysis and Calorimetry
Volume/Issue:
Volume 96: Issue 2
Thermal study of an epoxy system DGEBA (n=0)/mXDA modified with POSS
Authors:
M. Villanueva Universidade de Santiago de Compostela Campus Sur Research Group TERBIPROMAT, Departamento de Física Aplicada 15782 Santiago de Compostela Spain

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J. Martín-Iglesias Universidade de Santiago de Compostela Campus Sur Research Group TERBIPROMAT, Departamento de Física Aplicada 15782 Santiago de Compostela Spain

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J. Rodríguez-Añón Universidade de Santiago de Compostela Campus Sur Research Group TERBIPROMAT, Departamento de Física Aplicada 15782 Santiago de Compostela Spain

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J. Proupín-Castiñeiras Universidade de Santiago de Compostela Campus Sur Research Group TERBIPROMAT, Departamento de Física Aplicada 15782 Santiago de Compostela Spain

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Pages:
575–582
Online Publication Date:
13 Jan 2009
Publication Date:
01 May 2009
Article Category:
Research Article
DOI:
https://doi.org/10.1007/s10973-008-9213-x
Keywords:
activation energy; DSC; epoxy resin; glass transition temperature; polyhedral oligomeric silsesquioxanes nanoparticles; TG
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Abstract  

The thermal degradation of the epoxy system diglycidyl ether of bisphenol A (DGEBA n=0) and m-xylylenediamine (mXDA) containing different concentrations of polyhedral oligomeric silsesquioxanes (POSS) nanoparticles was studied by thermogravimetric analysis in order to determine the influence of both, the POSS concentration and the curing cycle on the degradation process and to compare it with the results for the non modified system. Glass transition temperatures for the same systems were also determined by differential scanning calorimetry. Different behaviors have been observed, depending on the POSS concentration and on the curing selection.

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Cover Journal of Thermal Analysis and Calorimetry
Journal of Thermal Analysis and Calorimetry
Print ISSN:
1388-6150
Online ISSN:
1572-8943

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Journal of Thermal Analysis and Calorimetry
Language English
Size A4
Year of
Foundation		 1969
Volumes
per Year		 1
Issues
per Year		 24
Founder Akadémiai Kiadó
Founder's
Address		 H-1117 Budapest, Hungary 1516 Budapest, PO Box 245.
Publisher Akadémiai Kiadó
Springer Nature Switzerland AG
Publisher's
Address		 H-1117 Budapest, Hungary 1516 Budapest, PO Box 245.
CH-6330 Cham, Switzerland Gewerbestrasse 11.
Responsible
Publisher		 Chief Executive Officer, Akadémiai Kiadó
ISSN 1388-6150 (Print)
ISSN 1588-2926 (Online)

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