Journal of Thermal Analysis and Calorimetry
Volume/Issue:
Volume 97: Issue 1
Thermal analysis applied in the crystallization study of SrSnO3
Authors:
Mary Alves Universidade Federal da Paraíba LACOM, Departamento de Química/CCEN Campus I João Pessoa PB Brazil

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Soraia Souza Universidade Federal da Paraíba LACOM, Departamento de Química/CCEN Campus I João Pessoa PB Brazil

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Márcia Silva Universidade Federal da Paraíba LACOM, Departamento de Química/CCEN Campus I João Pessoa PB Brazil

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Elaine Paris Universidade Federal da Paraíba LACOM, Departamento de Química/CCEN Campus I João Pessoa PB Brazil

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S. Lima UFPB LSR, Departamento de Engenharia Mecânica/CT Campus I João Pessoa PB 58059-900 Brazil

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R. Gomes UFPB LSR, Departamento de Engenharia Mecânica/CT Campus I João Pessoa PB 58059-900 Brazil

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E. Longo UNESP CMDMC—LIEC, Instituto de Química Araraquara SP Brazil

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A. de Souza Universidade Federal da Paraíba LACOM, Departamento de Química/CCEN Campus I João Pessoa PB Brazil

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Iêda Garcia dos Santos Universidade Federal da Paraíba LACOM, Departamento de Química/CCEN Campus I João Pessoa PB Brazil

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Pages:
179–183
Online Publication Date:
05 Aug 2009
Publication Date:
01 Jul 2009
Article Category:
Research Article
DOI:
https://doi.org/10.1007/s10973-009-0242-x
Keywords:
Stannate; Perovskite; Polymeric precursor method; Pechini; SrSnO3
Restricted access

Abstract  

SrSnO3 was synthesized by the polymeric precursor method with elimination of carbon in oxygen atmosphere at 250 °C for 24 h. The powder precursors were characterized by TG/DTA and high temperature X-ray diffraction (HTXRD). After calcination at 500, 600 and 700 °C for 2 h, samples were evaluated by X-ray diffraction (XRD), infrared spectroscopy (IR) and Rietveld refinement of the XRD patterns for samples calcined at 900, 1,000 and 1,100 °C. During thermal treatment of the powder precursor ester combustion was followed by carbonate decomposition and perovskite crystallization. No phase transition was observed as usually presented in literature for SrSnO3 that had only a rearrangement of SnO6 polyhedra.

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Cover Journal of Thermal Analysis and Calorimetry
Journal of Thermal Analysis and Calorimetry
Print ISSN:
1388-6150
Online ISSN:
1572-8943

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Journal of Thermal Analysis and Calorimetry
Language English
Size A4
Year of
Foundation		 1969
Volumes
per Year		 1
Issues
per Year		 24
Founder Akadémiai Kiadó
Founder's
Address		 H-1117 Budapest, Hungary 1516 Budapest, PO Box 245.
Publisher Akadémiai Kiadó
Springer Nature Switzerland AG
Publisher's
Address		 H-1117 Budapest, Hungary 1516 Budapest, PO Box 245.
CH-6330 Cham, Switzerland Gewerbestrasse 11.
Responsible
Publisher		 Chief Executive Officer, Akadémiai Kiadó
ISSN 1388-6150 (Print)
ISSN 1588-2926 (Online)

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