Authors:
Mary AlvesUniversidade Federal da Paraíba LACOM, Departamento de Química/CCEN Campus I João Pessoa PB Brazil

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Soraia SouzaUniversidade Federal da Paraíba LACOM, Departamento de Química/CCEN Campus I João Pessoa PB Brazil

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Márcia SilvaUniversidade Federal da Paraíba LACOM, Departamento de Química/CCEN Campus I João Pessoa PB Brazil

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Elaine ParisUniversidade Federal da Paraíba LACOM, Departamento de Química/CCEN Campus I João Pessoa PB Brazil

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S. LimaUFPB LSR, Departamento de Engenharia Mecânica/CT Campus I João Pessoa PB 58059-900 Brazil

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R. GomesUFPB LSR, Departamento de Engenharia Mecânica/CT Campus I João Pessoa PB 58059-900 Brazil

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E. LongoUNESP CMDMC—LIEC, Instituto de Química Araraquara SP Brazil

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A. de SouzaUniversidade Federal da Paraíba LACOM, Departamento de Química/CCEN Campus I João Pessoa PB Brazil

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Iêda Garcia dos SantosUniversidade Federal da Paraíba LACOM, Departamento de Química/CCEN Campus I João Pessoa PB Brazil

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Abstract  

SrSnO3 was synthesized by the polymeric precursor method with elimination of carbon in oxygen atmosphere at 250 °C for 24 h. The powder precursors were characterized by TG/DTA and high temperature X-ray diffraction (HTXRD). After calcination at 500, 600 and 700 °C for 2 h, samples were evaluated by X-ray diffraction (XRD), infrared spectroscopy (IR) and Rietveld refinement of the XRD patterns for samples calcined at 900, 1,000 and 1,100 °C. During thermal treatment of the powder precursor ester combustion was followed by carbonate decomposition and perovskite crystallization. No phase transition was observed as usually presented in literature for SrSnO3 that had only a rearrangement of SnO6 polyhedra.

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Journal of Thermal Analysis and Calorimetry
Language English
Size A4
Year of
Foundation
1969
Volumes
per Year
1
Issues
per Year
24
Founder Akadémiai Kiadó
Founder's
Address
H-1117 Budapest, Hungary 1516 Budapest, PO Box 245.
Publisher Akadémiai Kiadó
Springer Nature Switzerland AG
Publisher's
Address
H-1117 Budapest, Hungary 1516 Budapest, PO Box 245.
CH-6330 Cham, Switzerland Gewerbestrasse 11.
Responsible
Publisher
Chief Executive Officer, Akadémiai Kiadó
ISSN 1388-6150 (Print)
ISSN 1588-2926 (Online)

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