Abstract
A cellulose xanthate supported palladium(0) complex was synthesized using a simple method and characterized by XPS, TG/DTA etc. The complex has good thermal stability from room temperature to 250 °C and it was found to be an efficient catalyst for the Heck reaction of acrylic acid or styrene with aryl iodide at low temperature under atmospheric pressure, and the substituted trans-cinnamic acid or 1, 2-stilbene was obtained with high yield at 90 °C. The reaction duration is about 8 h. The cellulose xanthate supported palladium(0) complex could be separated from the reaction mixture easily and reused for several cycles. The yield of the product was up to 55.3% when the catalyst was run for 10 times. The active center in the complex is Pd metal.
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| Reaction Kinetics, Mechanisms and Catalysis | |
|---|---|
| Language | English |
| Size | B5 |
| Year of Foundation |
1974 |
| Volumes per Year |
1 |
| Issues per Year |
6 |
| Founder | Akadémiai Kiadó |
| Founder's Address |
H-1117 Budapest, Hungary 1516 Budapest, PO Box 245. |
| Publisher | Akadémiai Kiadó Springer Nature Switzerland AG |
| Publisher's Address |
H-1117 Budapest, Hungary 1516 Budapest, PO Box 245. CH-6330 Cham, Switzerland Gewerbestrasse 11. |
| Responsible Publisher |
Chief Executive Officer, Akadémiai Kiadó |
| ISSN | 1878-5190 (Print) |
| ISSN | 1878-5204 (Online) |
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