Reaction Kinetics, Mechanisms and Catalysis
Volume/Issue:
Volume 104: Issue 1
Preparation and properties of zirconia nanotube-supported zirconium sulfate catalyst
Authors:
Xixin Wang School of Material Science and Engineering, Hebei University of Technology, Tianjin 300130, People's Republic of China

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Jianling Zhao School of Material Science and Engineering, Hebei University of Technology, Tianjin 300130, People's Republic of China

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Xiaorui Hou School of Material Science and Engineering, Hebei University of Technology, Tianjin 300130, People's Republic of China

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Fang Wang School of Material Science and Engineering, Hebei University of Technology, Tianjin 300130, People's Republic of China

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Chengchun Tang School of Material Science and Engineering, Hebei University of Technology, Tianjin 300130, People's Republic of China

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Pages:
227–234
Online Publication Date:
01 Jul 2011
Publication Date:
01 Oct 2011
Article Category:
Research Article
DOI:
https://doi.org/10.1007/s11144-011-0344-x
Keywords:
ZrO2 nanotube; Zirconium sulfate; Supported catalyst
Restricted access

Abstract

ZrO2 nanotube arrays were prepared by the anodization method in a mixture of formamide and glycerol (volume ratio = 1:1) containing 1 wt% NH4F and 1 wt% H2O. The catalysts were obtained through the impregnation of zirconia nanotubes with zirconium sulfate aqueous solution followed by calcinating in air at high temperature. The morphology and structure of the nanotubes and catalysts were characterized through scanning electron microscopy, X-ray diffraction, and infrared spectra analysis. Various factors that affect the catalytic activity were investigated in detail. An esterification conversion percentage of 97.6% was achieved for the catalyst prepared with zirconia supports which were pretreated at 500 °C, followed by loading 65% Zr(SO4)2 and calcinating at 400 °C.

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Cover Reaction Kinetics, Mechanisms and Catalysis
Reaction Kinetics, Mechanisms and Catalysis
Print ISSN:
1878-5190
Online ISSN:
1878-5204

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Reaction Kinetics, Mechanisms and Catalysis
Language English
Size B5
Year of
Foundation		 1974
Volumes
per Year		 1
Issues
per Year		 6
Founder Akadémiai Kiadó
Founder's
Address		 H-1117 Budapest, Hungary 1516 Budapest, PO Box 245.
Publisher Akadémiai Kiadó
Springer Nature Switzerland AG
Publisher's
Address		 H-1117 Budapest, Hungary 1516 Budapest, PO Box 245.
CH-6330 Cham, Switzerland Gewerbestrasse 11.
Responsible
Publisher		 Chief Executive Officer, Akadémiai Kiadó
ISSN 1878-5190 (Print)
ISSN 1878-5204 (Online)

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