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K. Kuśmierek
K. Kuśmierek
Institute of Chemistry, Military University of Technology, 2 Kaliskiego Str., 00-908, Warsaw, Poland
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E. Bald
E. Bald
Department of Environmental Chemistry, University of Lodz, 163 Pomorska Str., 90-236, Lodz, Poland
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Summary
High-performance liquid chromatography has been used for measurement of the concentrations of total cysteine and cysteinylglycine in human urine. The method involved conversion of disulfides to their reduced counterparts by use of tris(2-carboxyethyl)phosphine hydrochloride, derivatization with 1-benzyl-2-chloropyridinium bromide, and ion-pairing reversed-phase high-performance liquid chromatographic separation with ultraviolet detection at 315 nm. The linearity of the method was validated in the ranges 50–300 and 5–50 µmol L−1 urine for cysteine and cysteinylglycine, respectively; regression coefficients were better than 0.999. The detection and quantitation limits were 0.2 and 0.5 µmol L−1, respectively, for both analytes. Intra-assay and inter-assay imprecision were below 6.0%, and accuracy was 98.95–100.80%. The method was applied to urine samples donated by apparently healthy volunteers.
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[1]. A. Pastore R. Massoud C. Motti A. Lo Russo G. Fucci C. Cortese G. Federici 1998 Clin. Chem. 44 825.
-
[2]. K. Kuśmierek R. Głowacki E. Bald 2006 Anal. Bioanal. Chem. 385 855.
-
[3]. K. Kuśmierek E. Bald 2008 Chromatographia 67 23.
-
[4]. K. Kuśmierek G. Chwatko E. Bald 2008 Chromatographia 68 S91.
-
[5]. D.M. Townsend K.D. Kew H. Tapiero 2004 Biomed. Pharmacother. 58 47.
-
[6]. D. Joly P. Rieu A. Mejean M.F. Gagnadoux M. Daudon P. Jungers 1999 Pediatr. Nephrol. 13 945.
-
[7]. B. Rojkovich E. Nagy T. Prohle G. Poor P. Gergely 1999 Clin. Diagn. Lab. Immunol. 6 683.
-
[8]. A. Hernaz A. Plaza E. Martin-Mola E. DeMiguel 1999 Clin. Biochem. 32 65.
-
[9]. C. Zhao J. Zhang J. Song 2001 Anal. Biochem. 297 170.
-
[10]. P. Lochman T. Adam D. Friedecky E. Hlidkova Z. Skopkova 2003 Electrophoresis 24 1200.
-
[11]. M. Wroński 1996 J. Chromatogr. B 676 29.
-
[12]. U. Hannestad B. Sorbo 1979 Clin. Chim. Acta 95 189.
-
[13]. X. Huang T.W. Kok 1991 J. Liq. Chromatogr. 14 2207.
-
[14]. B. Kagedal M. Kallberg 1984 J. Chromatogr. B. 308 75.
-
[15]. T. Fiskerstrand H. Refsum G. Kvalheim P.M. Ueland 1993 Clin. Chem. 39 263.
-
[16]. P. Ventura R. Panini M.C. Pasini G. Scarpetta G. Savioli 1999 Pharmacol. Res. 40 345.
-
[17]. I. Fermo C. Arcelloni R. Paroni 2002 Anal. Biochem. 307 181.
-
[18]. S.C. Liang H. Wang Z.M. Zhang H.S. Zhang 2005 Anal. Bioanal. Chem. 381 1100.
-
[19]. E. Kaniowska G. Chwatko R. Głowacki P. Kubalczyk E. Bald 1998 J. Chromatogr. A 798 27.
-
[20]. E. Bald R. Głowacki J. Drzewoski 2001 J. Chromatogr. A 913 319.
-
[21]. K. Amarnath V. Amarnath K. Amarnath H.L. Valentine W.M. Valentine 2003 Talanta 60 1229.
-
[22]. M.J. Magera J.M. Lacey B. Casetta P. Rinaldo 1999 Clin. Chem. 45 1517.
-
[23]. J.E. Wear B.G. Keevil 2005 Clin. Chem. 51 787.
-
[24]. G. Weaving B.F. Rocks S.A. Iversen M.A. Titheradge 2006 Ann. Clin. Biochem. 43 474.
-
[25]. B. Seiwert U. Karst 2007 Anal. Chem. 79 7131.
-
[26]. E. Bald S. Sypniewski J. Drzewoski M. Stępień 1996 J. Chromatogr. B 681 283.
-
[27]. E. Bald S. Sypniewski 1997 Fresenius' J. Anal. Chem. 328 554.
-
[28]. V.P. Shah K.K. Midha S. Dighe I.J. McGilveray J.P. Skelly A. Yacobi T. Layloff C.T. Viswanathan C.E. Cook R.D. McDowall K.A. Pittman S. Spector 1992 Int. J. Pharm. 82 1.
-
[29]. FDA Guidance for Industry Bioanalytical Method Validation, http://www.fda.gov/cder/guidance/4252fnl.pdf.
Senior editors
Editor(s)-in-Chief: Sajewicz, Mieczyslaw, University of Silesia, Katowice, Poland
Editors(s)
- Danica Agbaba, University of Belgrade, Belgrade, Serbia (1953-2024)
- Łukasz Komsta, Medical University of Lublin, Lublin, Poland
- Ivana Stanimirova-Daszykowska, University of Silesia, Katowice, Poland
- Monika Waksmundzka-Hajnos, Medical University of Lublin, Lublin, Poland
Editorial Board
- Ravi Bhushan, The Indian Institute of Technology, Roorkee, India
- Jacek Bojarski, Jagiellonian University, Kraków, Poland
- Bezhan Chankvetadze, State University of Tbilisi, Tbilisi, Georgia
- Michał Daszykowski, University of Silesia, Katowice, Poland
- Tadeusz H. Dzido, Medical University of Lublin, Lublin, Poland
- Attila Felinger, University of Pécs, Pécs, Hungary
- Kazimierz Glowniak, Medical University of Lublin, Lublin, Poland
- Bronisław Glód, Siedlce University of Natural Sciences and Humanities, Siedlce, Poland
- Anna Gumieniczek, Medical University of Lublin, Lublin, Poland
- Urszula Hubicka, Jagiellonian University, Kraków, Poland
- Krzysztof Kaczmarski, Rzeszow University of Technology, Rzeszów, Poland
- Huba Kalász, Semmelweis University, Budapest, Hungary
- Katarina Karljiković Rajić, University of Belgrade, Belgrade, Serbia
- Imre Klebovich, Semmelweis University, Budapest, Hungary
- Angelika Koch, Private Pharmacy, Hamburg, Germany
- Piotr Kus, Univerity of Silesia, Katowice, Poland
- Debby Mangelings, Free University of Brussels, Brussels, Belgium
- Emil Mincsovics, Corvinus University of Budapest, Budapest, Hungary
- Ágnes M. Móricz, Centre for Agricultural Research, Budapest, Hungary
- Gertrud Morlock, Giessen University, Giessen, Germany
- Anna Petruczynik, Medical University of Lublin, Lublin, Poland
- Robert Skibiński, Medical University of Lublin, Lublin, Poland
- Bernd Spangenberg, Offenburg University of Applied Sciences, Germany
- Tomasz Tuzimski, Medical University of Lublin, Lublin, Poland
- Adam Voelkel, Poznań University of Technology, Poznań, Poland
- Beata Walczak, University of Silesia, Katowice, Poland
- Wiesław Wasiak, Adam Mickiewicz University, Poznań, Poland
- Igor G. Zenkevich, St. Petersburg State University, St. Petersburg, Russian Federation
SAJEWICZ, MIECZYSLAW
E-mail:mieczyslaw.sajewicz@us.edu.pl
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| 2023 | |
|---|---|
| Web of Science | |
| Journal Impact Factor | 1.7 |
| Rank by Impact Factor | Q3 (Chemistry, Analytical) |
| Journal Citation Indicator | 0.43 |
| Scopus | |
| CiteScore | 4.0 |
| CiteScore rank | Q2 (General Chemistry) |
| SNIP | 0.706 |
| Scimago | |
| SJR index | 0.344 |
| SJR Q rank | Q3 |
| Acta Chromatographica | |
|---|---|
| Publication Model | Online only Gold Open Access |
| Submission Fee | none |
| Article Processing Charge | 400 EUR/article Effective from 1st Feb 2025: 700 EUR/article |
| Regional discounts on country of the funding agency | World Bank Lower-middle-income economies: 50% World Bank Low-income economies: 100% |
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| Subscription Information | Gold Open Access |
| Purchase per Title | |
| Acta Chromatographica | |
|---|---|
| Language | English |
| Size | A4 |
| Year of Foundation |
1988 |
| Volumes per Year |
1 |
| Issues per Year |
4 |
| Founder | Institute of Chemistry, University of Silesia |
| Founder's Address |
PL-40-007 Katowice, Poland, Bankowa 12 |
| Publisher | Akadémiai Kiadó |
| Publisher's Address |
H-1117 Budapest, Hungary 1516 Budapest, PO Box 245. |
| Responsible Publisher |
Chief Executive Officer, Akadémiai Kiadó |
| ISSN | 2083-5736 (Online) |
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