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  • 1 Department of Analytical Chemistry and Pharmaceutical Technology, Pharmaceutical Institute, Vrije Universiteit Brussel - VUB, Laarbeeklaan 103, 1090, Brussels, Belgium
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Summary

A liquid chromatographic fingerprinting methodology has been established for identification and quality control of traditional herbal medicines. The methodology was developed from four case studies. Samples of Herba Artemisia annua, Herba Artemisia scoparia, Rhizoma Ligusticum chuanxiong (also called Rhizoma chuanxiong), and Rhizoma Ligusticum jeholense (also called Rhizoma ligustici) were investigated. In each case study, sample preparation and chromatographic conditions (column, organic modifier, column temperature, detection wavelength, and mechanism) were varied to obtain good fingerprints, i.e. with the maximum number of peaks. Further optimization was then performed either by reducing the analysis time or increasing efficiency. The case studies led to the development of a general methodology consisting of sample preparation and HPLC fingerprint development. The fingerprints obtained with the developed methodology were then successfully used to distinguish between the two Artemisia species and between the two Ligusticum species. The methodology also was used to obtain fingerprints for a large number of different Vietnamese Mallotus species, and for Citri reticulatae pericarpium samples collected in different regions of China.

  • [1]. C. Aschwanden 2001 Bull. World Health Organ. 79 691692.

  • [2]. Y.-Z. Liang P. Xie K. Chan 2004 J. Chromatogr. B 812 5370.

  • [3]. S. Bent R. Ko 2004 Am. J. Med. 116 478485.

  • [4]. R. Bauer 1998 Drug Inf. J. 32 101110.

  • [5]. V.E. Tyler 1999 J. Nat. Prod. 62 15891592.

  • [6]. G.B. Mahady H.H.S. Fong N.R. Farnsworth 2001 Botanical Dietary Supplements: Quality, Safety and Efficacy Swets and Zeitlinger Lisse, The Netherlands.

    • Search Google Scholar
    • Export Citation
  • [7]. A.M. van Nederkassel C.J. Xu P. Lancelin M. Sarraf D.A. MacKenzie N.J. Walton F. Bensaid M. Lees G.J. Martin J.R. Desmurs D.L. Massart J. Smeyers-Verbeke Y. Vander Heyden 2006 J. Chromatogr. A 1120 291298.

    • Search Google Scholar
    • Export Citation
  • [8]. N. Nguyen Hoai B. Dejaegher C. Tistaert V. Nguyen Thi Hong C. Rivière G. Chataigné M. Van Chau J. Quetin-Leclercq Y. Vander Heyden 2009 J. Pharm. Biomed. Anal. 50 753763.

    • Search Google Scholar
    • Export Citation
  • [9]. K.M. Wu J.G. Farrelly R. Upton J. Chen 2007 Phytomedicine 14 273279.

  • [10]. C. Han J. Chen B. Chen F. Sen-Chun Lee X. Wang 2006 J. Sep. Sci. 29 21972202.

  • [11]. L.-S. Wu J.-P. Si X.-Q. Yuan X.-R. Shi 2009 Chin. J. Nat. Med. 7 4046.

  • [12]. A.M. van Nederkassel M. Daszykowski D.L. Massart Y. Vander Heyden 2005 J. Chromatogr. A 1096 177186.

  • [13]. M. Daszykowski Y. Vander Heyden B. Walczak 2007 J. Chromatogr. A 1176 1218.

  • [14]. M. Dumarey A.M. van Nederkassel E. Deconinck Y. Vander Heyden 2008 J. Chromatogr. A 1192 8188.

  • [15]. Pharmacopoeia of the People's Republic of China, Volume 1, Chinese Pharmacopoeia Commission, Peoples Medical Publishing House, 2005.

    • Search Google Scholar
    • Export Citation
  • [16]. Guidelines for the Assessment of Herbal Medicine, World Health Organization, Munich, Germany, 1991, http://www.who.int/en (accessed February 22, 2010).

    • Search Google Scholar
    • Export Citation
  • [17]. WHO, General Guidelines for Methodologies on Research and Evaluation of Traditional Medicines, Geneva, 2000, http://www.who.int (accessed February 22, 2010).

    • Search Google Scholar
    • Export Citation
  • [18]. Drug Administration Bureau of China, Requirements for Studying Fingerprints of Traditional Chinese Medicine Injection, Drug Administration Bureau of China, Beijing, China, 2002.

    • Search Google Scholar
    • Export Citation
  • [19]. Food and Drug Administration, Guidance for Industry: Botanical Drug Products, Food and Drug Administration, June 2004, p. 10, http://www.fda.gov/cder/guidance/4592fnl.pdf (accessed March 23, 2009).

    • Search Google Scholar
    • Export Citation
  • [20]. CHMP, Guideline on quality of herbal medicinal products/traditional herbal medicinal products. Committee for medicinal products for human use (CHMP), European Medicines Agency Inspections, July 21, 2005, CPMP/QWP/2819/00 Rev 1, EMEA/CVMP/814/00 Rev 1, http://www.emea.europa.eu/home.htm (accessed February 22, 2010).

    • Search Google Scholar
    • Export Citation
  • [21]. D.L. Massart B.G.M. Vandeginste L.M.C. Buydens S. De Jong P.J. Lewi J. Smeyers-Verbeke 1997 Handbook of Chemometrics and Qualimetrics: Part A Elsevier Amsterdam.

    • Search Google Scholar
    • Export Citation
  • [22]. E. Morgan 1991 Chemometrics: Experimental Design, Analytical Chemistry by Open Learning Wiley Chichester.

  • [23]. D.C. Montgomery 1997 Design and analysis of experiments 4th edn J. Wiley New York.

  • [24]. Y. Vander Heyden C. Perrin D.L. Massart 2000 Optimization Strategies for HPLC and CZE K. Valko Handbook of Analytical Separations 1, Separation Methods in Drug Synthesis and Purification Elsevier Amsterdam 163212.

    • Search Google Scholar
    • Export Citation
  • [25]. A.M. van Nederkassel V. Vijverman D.L. Massart Y. Vander Heyden 2005 J. Chromatogr. A 1085 230239.

  • [26]. G. Alaerts N. Matthijs J. Smeyers-Verbeke Y. Vander Heyden 2007 J. Chromatogr. A 1172 18.

  • [27]. Y. Li K. Bi 2003 Biomed. Chromatogr. 17 543546.

  • [28]. S. Mathew T.E. Abraham 2004 Crit. Rev. Biotechnol. 24 5983.

  • [29]. H. Priefert J. Rabenhorst A. Steinbüchel 2001 Appl. Microbiol. Biotechnol. 56 296314.

  • [30]. F.C. Sánchez S.C. Rutan M.D. G. García D.L. Massart 1997 Chemometr. Intell. Lab. Syst. 36 153164.

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Senior editors

Editor(s)-in-Chief: Kowalska, Teresa

Editor(s)-in-Chief: Sajewicz, Mieczyslaw

Editors(s) Danica Agbaba (University of Belgrade, Belgrade, Serbia);
Ivana Stanimirova-Daszykowska (University of Silesia, Katowice, Poland),
Monika Waksmundzka-Hajnos (Medical University of Lublin, Lublin, Poland)

Editorial Board

R. Bhushan (The Indian Institute of Technology, Roorkee, India)
J. Bojarski (Jagiellonian University, Kraków, Poland)
B. Chankvetadze (State University of Tbilisi, Tbilisi, Georgia)
M. Daszykowski (University of Silesia, Katowice, Poland)
T.H. Dzido (Medical University of Lublin, Lublin, Poland)
A. Felinger (University of Pécs, Pécs, Hungary)
K. Glowniak (Medical University of Lublin, Lublin, Poland)
B. Glód (Siedlce University of Natural Sciences and Humanities, Siedlce, Poland)
K. Kaczmarski (Rzeszow University of Technology, Rzeszów, Poland)
H. Kalász (Semmelweis University, Budapest, Hungary)
I. Klebovich (Semmelweis University, Budapest, Hungary)
A. Koch (Private Pharmacy, Hamburg, Germany)
Ł. Komsta (Medical University of Lublin, Lublin, Poland)
P. Kus (Univerity of Silesia, Katowice, Poland)
D. Mangelings (Free University of Brussels, Brussels, Belgium)
E. Mincsovics (Corvinus University of Budapest, Budapest, Hungary)
G. Morlock (Giessen University, Giessen, Germany)
J. Sherma (Lafayette College, Easton, PA, USA)
R. Skibiński (Medical University of Lublin, Lublin, Poland)
B. Spangenberg (Offenburg University of Applied Sciences, Germany)
T. Tuzimski (Medical University of Lublin, Lublin, Poland)
Y. Vander Heyden (Free University of Brussels, Brussels, Belgium)
A. Voelkel (Poznań University of Technology, Poznań, Poland)
B. Walczak (University of Silesia, Katowice, Poland)
W. Wasiak (Adam Mickiewicz University, Poznań, Poland)

KOWALSKA, TERESA
E-mail: kowalska@us.edu.pl

SAJEWICZ, MIECZYSLAW
E-mail:msajewic@us.edu.pl

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2020
 
Total Cites
650
WoS
Journal
Impact Factor
1,639
Rank by
Chemistry, Analytical 71/83 (Q4)
Impact Factor
 
Impact Factor
1,412
without
Journal Self Cites
5 Year
1,301
Impact Factor
Journal
0,34
Citation Indicator
 
Rank by Journal
Chemistry, Analytical 75/93 (Q4)
Citation Indicator
 
Citable
45
Items
Total
43
Articles
Total
2
Reviews
Scimago
28
H-index
Scimago
0,316
Journal Rank
Scimago
Chemistry (miscellaneous) Q3
Quartile Score
 
Scopus
393/181=2,2
Scite Score
 
Scopus
General Chemistry 215/398 (Q3)
Scite Score Rank
 
Scopus
0,560
SNIP
 
Days from
58
sumbission
 
to acceptance
 
Days from
68
acceptance
 
to publication
 
Acceptance
51%
Rate

2019  
Total Cites
WoS
495
Impact Factor 1,418
Impact Factor
without
Journal Self Cites
1,374
5 Year
Impact Factor
0,936
Immediacy
Index
0,460
Citable
Items
50
Total
Articles
50
Total
Reviews
0
Cited
Half-Life
6,2
Citing
Half-Life
8,3
Eigenfactor
Score
0,00048
Article Influence
Score
0,164
% Articles
in
Citable Items
100,00
Normalized
Eigenfactor
0,05895
Average
IF
Percentile
20,349
Scimago
H-index
26
Scimago
Journal Rank
0,255
Scopus
Scite Score
226/167=1,4
Scopus
Scite Score Rank
Chemistry (miscellaneous) 240/398 (Q3)
Scopus
SNIP
0,494
Acceptance
Rate
41%

 

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Acta Chromatographica
Language English
Size A4
Year of
Foundation
1992
Publication
Programme
2021 Volume 33
Volumes
per Year
1
Issues
per Year
4
Founder Institute of Chemistry, University of Silesia
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Address
PL-40-007 Katowice, Poland, Bankowa 12
Publisher Akadémiai Kiadó
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ISSN 0236-6290 (Print)
ISSN 2083-5736 (Online)

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