Journal of Flow Chemistry
Volume/Issue:
Volume 5: Issue 1
Catalytic Properties of Platinum Nanoparticles Obtained in a Single Step Simultaneous Reduction of Pt(IV) Ions and Graphene Oxide
Authors:
Marek Wojnicki AGH University of Science and Technology Faculty of Non-Ferrous Metals, Department of Physical Chemistry and Metallurgy of Non-Ferrous Metals al. A. Mickiewicza 30 30-059 Krakow Poland

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Magdalena Luty-Błocho AGH University of Science and Technology Faculty of Non-Ferrous Metals, Department of Physical Chemistry and Metallurgy of Non-Ferrous Metals al. A. Mickiewicza 30 30-059 Krakow Poland

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Krzysztof Mech Academic Centre for Materials and Nanotechnology AGH University of Science and Technology al. A. Mickiewicza 30 30-059 Krakow Poland

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Justyna Grzonka Faculty of Materials Science and Engineering Warsaw University of Technology ul. Wołoska 141 02-507 Warsaw Poland

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Krzysztof Fitzner AGH University of Science and Technology Faculty of Non-Ferrous Metals, Department of Physical Chemistry and Metallurgy of Non-Ferrous Metals al. A. Mickiewicza 30 30-059 Krakow Poland

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Krzysztof Kurzydłowski Faculty of Materials Science and Engineering Warsaw University of Technology ul. Wołoska 141 02-507 Warsaw Poland

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Pages:
22–30
Online Publication Date:
30 Jan 2015
Publication Date:
25 Mar 2015
Article Category:
Research Article
DOI:
https://doi.org/10.1556/jfc-d-14-00032
Keywords:
platinum nanoparticles; graphene oxide; microreactor; microflow reactor; deposition; DMAB; glucose electro-oxidation
Restricted access

A composite material consisting of metallic platinum nanoparticles and reduced graphene oxide was successfully obtained in microflow reactor. Moreover, subnanometric platinum particles were observed. Reduced graphene oxide plays an important role as a stabilizing agent for platinum nanoparticles. Reduced graphene oxide coverage and platinum particle size as well as size distribution depend mainly on initial concentration of platinum(IV) ions. High level of reduced graphene oxide coverage by platinum nanoparticles (PtNPs) was obtained and is equal to 71%. This in turn effects significantly the mass ratio of reduced graphene oxide to PtNPs which is equal to 49% (w/w). Fourier transform infrared (FT-IR) and X-ray photoelectron spectroscopy (XPS) analysis of the obtained materials were performed. Also, catalytic properties of the obtained composite material consisting of PtNPs at reduced graphene oxide surface, towards electrochemical glucose oxidation, were investigated. It was found that the studied materials exhibit high catalytic activity for glucose electro-oxidation process.

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Cover Journal of Flow Chemistry
Journal of Flow Chemistry A Journal of the Flow Chemistry Society
Print ISSN:
2062-249X
Online ISSN:
2063-0212

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Journal of Flow Chemistry
Language English
Size A4
Year of
Foundation		 2011
Volumes
per Year		 1
Issues
per Year		 4
Founder Áramlásos Kémiai Tudományos Társaság
Founder's
Address		 H-1031 Budapest, Hungary Záhony utca 7.
Publisher Akadémiai Kiadó
Springer Nature Switzerland AG
Publisher's
Address		 H-1117 Budapest, Hungary 1516 Budapest, PO Box 245.
CH-6330 Cham, Switzerland Gewerbestrasse 11
Responsible
Publisher		 Chief Executive Officer, Akadémiai Kiadó
ISSN 2062-249X (Print)
ISSN 2063-0212 (Online)

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