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M.Y. Guida
myassineguida@gmail.com
https://orcid.org/0000-0002-5841-5271
M.Y. Guida
Organic Chemistry and Analytical Laboratory (LCOA), Faculty of Sciences and Techniques (FST), University of Sultan Moulay Slimane (USMS), 23000 Béni-Mellal , Morocco
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S.E. Lanaya
S.E. Lanaya
Organic Chemistry and Analytical Laboratory (LCOA), Faculty of Sciences and Techniques (FST), University of Sultan Moulay Slimane (USMS), 23000 Béni-Mellal , Morocco
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F.E. Laghchioua
F.E. Laghchioua
Organic Chemistry and Analytical Laboratory (LCOA), Faculty of Sciences and Techniques (FST), University of Sultan Moulay Slimane (USMS), 23000 Béni-Mellal , Morocco
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Z. Rbihi
Z. Rbihi
Organic Chemistry and Analytical Laboratory (LCOA), Faculty of Sciences and Techniques (FST), University of Sultan Moulay Slimane (USMS), 23000 Béni-Mellal , Morocco
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A. Hannioui
A. Hannioui
Organic Chemistry and Analytical Laboratory (LCOA), Faculty of Sciences and Techniques (FST), University of Sultan Moulay Slimane (USMS), 23000 Béni-Mellal , Morocco
Department of Chemistry and Environment, Faculty of Sciences and Techniques (FST), University of Sultan Moulay Slimane (USMS), 23000Béni-Mellal , Morocco
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Department of Chemistry and Environment, Faculty of Sciences and Techniques (FST), University of Sultan Moulay Slimane (USMS), 23000
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Abstract
This study deals with fast pyrolysis of sawdust wood waste (SWW) at the range of temperature 300–700 °C in a stainless steel tubular reactor. The aim was to experimentally investigate how the temperature, the particle size, the nitrogen flow rate (N2) and the heating rate affect bio-oil, bio-char and gaseous products. These parameters were varied in the ranges of 5–20 °C/min, below 0.1–1.5 mm and 20–200 mL min−1, respectively. It was concluded that both the temperature and heating rate have a significant effect on both yield of bio-oil and bio-char resulting from pyrolysis of SWW. The liquid products obtained at various pyrolysis temperatures were subjected into column chromatography after removal of asphaltenes (hexane insoluble). Obtained bio-oils (maltenes or hexane soluble) were classified as aliphatic, aromatic and polar sub-fractions. The maximum of bio-oil yield of 39.5 wt% was obtained at a pyrolysis temperature of 500 °C, particle size between 0.5 and 1 mm, nitrogen flow rate (N2) of 100 mL min−1 and heating rate of 5 °C/min. Liquid product (bio-oil) obtained under the most suitable and optimal condition was characterized by elemental analysis, Nuclear magnetic resonance spectroscopy (1H NMR and 13C NMR), Fourier transformed infrared spectroscopy (FT-IR). The analysis of liquid showed that bio-oil from SWW could be a potential source of renewable fuel production and value added chemical. The yield of char generally decreases with increasing the temperature, the char yield passes from 54.61 to 29.47 wt% at the heating rate of 5 °C/min and from 50.01 to 24.5 wt% at the heating rate of 20 °C/min at the same range of temperature (300–700 °C). Solid products (bio-char) obtained in the presence of nitrogen (N2) contain a very important percentage of carbon and high heating values (HHVs).
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Prof. Felföldi, József
Institute: MATE - Hungarian University of Agriculture and Life Sciences, Institute of Food Science and Technology, Department of Measurements and Process Control
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