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Agrokémia és Talajtan
Authors: Takács Tünde, Kelemen Bettina, Parádi István, Cseresnyés Imre, Mikó Péter, and Füzy Anna
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Agrokémia és Talajtan
Authors: Csontos Péter, Tamás Júlia, Kovács Zsófia, Schellenberger Judit, and Kalapos Tibor
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“Talaj – növény holobiont komplex – a megismeréstől az alkalmazásig”•

tudományos előadóülés (on-line), 2021. szeptember 16.

Agrokémia és Talajtan
Authors: Szili-Kovács Tibor and Márialigeti Károly
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Agrokémia és Talajtan
Authors: Szalai Zoltán, Ujházy Noémi, Megyes Melinda, Jakab Gergely, Madarász Balázs, Zacháry Dóra, Árendás Tamás, Barcza Zoltán, and Borsodi Andrea
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Abstract

As the world is facing numerous global ecological issues at once, the question arises of what will help mitigate and solve contemporary matters related to resource management or climate change without devastating the economies. Fortunately, the widespread application of the circular economy would help countries worldwide simultaneously ensure economic growth without significant environmental deterioration, essentially decoupling the two factors. While Hungary’s contribution to environmental problems is not significant in absolute terms, the economic sector’s circular transition could help the country decrease its impact in relative terms and pave the path for a green economy. Nevertheless, companies, especially SMEs, tend to struggle the most with the initial phases of the shift thus it is crucial to assess the factors that prevent and support their transition.

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Abstract

This study establishes a method for rapid detection of clonidine and cyproheptadine in foods of animal origin. In order to obtain the best detection method, capillary zone electrophoresis (CZE), large volume sample stacking (LVSS), and sweeping-micellar electrokinetic capillary chromatography (sweeping-MEKC) were used respectively. The limits of detection (LODs) of clonidine and cyproheptadine by LVSS-CZE were 0.028 μg mL−1 and 0.034 μg mL−1, and those by sweeping-MEKC were 0.023 μg mL−1 and 0.031 μg mL−1, respectively. Compared with the CZE method, the two online pre-concentration technologies have greatly improved the detection sensitivity and achieved good enrichment results. However, compared with the sweeping-MEKC system, the LVSS system consumed a longer time and was greatly affected by the actual sample matrix. The sweeping-MEKC method was proved to be suitable for real sample analysis. Under the best sweeping-MEKC conditions, clonidine and cyproheptadine could be well separated within 8 min and good linear relationships in the range of 0.1–1.0 μg mL−1 (r 2 > 0.99) were obtained. This method was successfully applied to the determination of clonidine and cyproheptadine in animal-derived foods with the recoveries of 82.3%–90.1% and the relative standard deviations (RSDs) less than 3.11%. The sweeping-MEKC method is simple to operate and has great potential in the rapid detection of clonidine and cyproheptadine in animal-derived foods.

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