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Spectral and thermal studies on copper(II) complexes of acenaphthaquinonemono(4-methylquinolinyl) hydrazone

Journal of Thermal Analysis and Calorimetry
Volume/Issue:
Volume 38: Issue 6
DOI:
https://doi.org/10.1007/bf01975076
Authors:
B. Garg
,
P. Singh
, and
S. Garg
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Thermal and magnetic studies of mixed ligand complexes of chromium(III) containing dithiocarbamate and acetylacetone/oxine/glycine moieties

Journal of Thermal Analysis and Calorimetry
Volume/Issue:
Volume 37: Issue 11-12
DOI:
https://doi.org/10.1007/bf01912799
Authors:
B. S. Garg
,
R. Dixit
,
A. L. Singh
, and
R. K. Sharma

Chromium(III) complexes of the type Cr(A)(A′)2, Cr(A)2(A′) and Cr(A)3 have been prepared (whereA is either piperidyldithiocarbamate or morpholyldithiocarbamate andA′ is glycine or oxine or acetylacetone moiety). The mixed ligand complexes have been charac terized by elemental analyses, magnetic susceptibility measurements and thermal studies. The complexes show magnetic moment in the range of 3.5–4.3 B.M. which corresponds to three unpaired electrons. TG studies have also been carried out, in order to study the mode of decomposition of the complexes and to evaluate various kinetic parameters.

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