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Acta Chromatographica
Authors:
Samiuela Lee
,
Christa E. Nath
,
Ben W. R. Balzer
,
Craig R. Lewis
,
Toby N. Trahair
,
Antoinette C. Anazodo
, and
Peter J. Shaw

oral alectinib capsules twice daily (Alecensa®, 600 mg). Lithium heparin blood samples (1–2 mL) were collected prior to the first alectinib dose, then at 0 min, 0.5 h, 1 h, 2 h, 4 h, 6 h, 12 h, and 24 h after the first dose, and then immediately prior

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procedure with L 1 . Yield: (76%) 4.71 g. Anal. calcd. for C 16 H 19 N 5 (281.36): C 68.3; H 6.8; N 24.9%. Found: C 68.5; H 6.9; N 25.1%. IR (KBr, cm −1 ): 3304 (NH), 3012 (Ar–CH), 2933–2835 (R-CH), 1653 (C=N), 1595(C=C). 1 H NMR (δ, ppm, CDCl 3 ): 8.53 (s

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Thermal decomposition of acrylamide from polyacrylamide

Time-resolved pyrolysis with ion-attachment mass spectrometry

Journal of Thermal Analysis and Calorimetry
Authors:
Yuki Kitahara
,
Ko Okuyama
,
Keita Ozawa
,
Takuya Suga
,
Seiji Takahashi
, and
Toshihiro Fujii

16 76 C 3 H 7 CN 17 77 C 4 H 6 O 12

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molecule is C 3 N 3 O 4 H 6 + ClO 4 − , which is made up of a cation C 3 N 3 O 4 H 6 + (DNAZ + ) and an anion ClO 4 − . The molecular structure and atom labeling are shown in Fig. 1 . Fig. 1 Molecular

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linearly increases with WC with respect to Δ KCN h (see arrows in Fig. 4 ). These points correspond to 74% WC ( t = 158 min, Δ h = −4.8 J g −1 ) for A7636RG ( Fig. 4A ), 57% WC ( t = 142 min, Δ h = −6.9 J g −1 ) for Munasqa ( Fig. 4B ), 33% WC ( t

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-5866(02)00078-3 . 4. Dunne , JA , Rao , M , Sircar , S , Gorte , RJ , Myers , AL . Calorimetric heats of adsorption and adsorption isotherms. 2. O 2 , N 2 , Ar, CO 2 , CH 4 , C 2 H 6 , and SF 6 on NaX, H-ZSM-5, and Na-ZSM-5

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,4′-dichloroazobenzene To a one-necked round-bottomed flask equipped with a mechanical stirrer, thermometer, and condenser, 2-chloro-4-(4-chloro-phenylazo)-phenol, NaOH (Fluka pellets 100%) and C 2 H 5 OH (Fluka absolute)–C 6 H 6 (Fluka 99%) mixture (3:1, in

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(pfed)]@ Mont ; Anal. Found: C, 4.26; H, 7.07; N, 1.41; C/N, 3.02 [calcd. C/N for net Cu(pfpd): 3.00]; % Cu (atomic absorption): 1.61; IR (KBr, cm −1 ): 1655 [ ν (C=N)]; DRS [d → d]: 439 nm. [Cu(pfpd)]@ Mont ; Anal. found: C, 4.21; H, 6.97; N, 1.34; C/N, 3

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–CH), 6.84–6.86 (d, 2H, Ar– H ), 6.91–6.93 (d, 2H, Ar– H ), 7.45–7.53 (d, 8H, Ar– H ). 8-[(4′-(( S )-2-Methylbutyloxy)-4-terphenyl)oxy]-1-octyne ( AM 6 OTPhOR ∗) Under the protection of nitrogen, 4-hydroxy-4

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.05(65) O6–H6···O12 0.820(9) 2.193(12) 2.910(16) 146.08(69) C22–H22···O9 0

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