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thermal characterization techniques are thermogravimetric analyzer (TG), differential thermal analyzer (DTA), differential scanning calorimeter (DSC), dynamical mechanical analyzer (DMA), and thermal constant analyzer (TCA) etc. Table 1 depicts the list

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Short course on thermal analysis October 15–17, 2012, Budapest, Hungary

Journal of Thermal Analysis and Calorimetry
Authors: J. Menczel and B. Androsits

mechanical analysis (DMA) local thermal analysis (micro- and nano-thermal analysis) coupled thermal analysis techniques The basic principles of each technique will be presented, followed by descriptions of the instrumentation and instruction on calibration

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the International Standards counterpart, ISO 75. It will then be discussed an alternative method for capturing a more complete picture of the effect, that temperature has on modulus. This technique, known as dynamic mechanical analysis (DMA) provides

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with the selected value of Hultgren. In 1989, in a report for NPL (DMA (A) 195), by Dinsdale [ 7 ], the selected value is 360 °C. This value is actually the one which is selected by SGTE (Scientific Group Thermodata Europe). In 1992, in ASM Handbook Vol

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of Poly (MAc- co -DMA- cl -MBAm) hydrogel immobilized Bacillus cereus MTCC 8372 lipase for synthesis of geranyl acetate. J. Appl. Polym. Sci. 110 , 837–846 (2008). Kanwar S. S

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analysis (DMA), three-point bending test, and Brinell’s hardness. The influence of poly(ester) structure on cross-linking density ( ν e ), tgδ max , tgδ max height, storage modulus ( ), hardness, flexural modulus at bending ( E mod ), deflection at

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hexamethylphosphotriamide (HMPA), tetrahydrofuran (THF), N , N -dimethylacetamide (DMA), 1,2-dimethoxyethane (1,2-DME), and 2-butanone as a function of the of mixed solvent composition exhibit maxima within the range of high water content. These maxima are related to a

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of oligoester HPTL32 was determined by the use of the cryoscopy method in Marcel OS3000 (Marcel Poland apparatus). 1,1,2,2 tetrabromoethane was used as the solvent. The DMTA spectra were recorded on analyzer Q800 DMA (TA Instruments). The

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conducted in DMSO, DMA, ethanol and methanol instead of DMF, similar results were obtained under same conditions (entries 6–9). It is worth noting that the reactions in aqueous alcohols gave excellent results which can be fascinating because the organic

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