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Kinetics of thermal degradation of poly(vinyl chloride)
Thermogravimetry and spectroscopy
. Thermochim Acta . 1992 ; 203 : 519 – 526 . 10.1016/0040-6031(92)85222-H . 50. Ortega , A . Some successes and failures of the methods based on several experiments . Thermochim Acta . 1996
. 0.000 Corrosion Corrosiveness to copper, 3 h, 50 °C – ASTM D 130 1 max. 1 b
-IR spectroscopy. Experimental section Paraffinic model systems The high molecular weight n -alkanes used in this study were obtained from Sigma-Aldrich with the following purity grades: tetracosane, C 24 H 50 (99
found (ng mL −1 , mean ± SD) Precision (%RSD) Accuracy (%) Bench top (up to 9 h) 5.0 4.7 ± 0
chromatography separation, limonin (C 26 H 30 O 8 ) and β-sitosterol (C 29 H 50 O) were extracted from the seeds and pulp of Citrus suavissima Hort. ex Tanaka , respectively [ 5 ]. Their structures were identified by spectral analysis ( 1 H NMR, 13 C NMR, DEPT
.6 ± 1.6 MRT (0−∞) h 7.2 ± 6.6 6.1 ± 2.5 t 1/2 z h 5.0 ± 3.0 3.5 ± 1.8 V z L/kg 35.9 ± 26.9 85.8 ± 23.6 CLz L/h/kg 6.0 ± 2.1 18.8 ± 6.9 C max ng/mL 90.2 ± 8.2 81.0 ± 12.4 Bioavailability 37.5% Conclusion In this study, a simple and fast UPLC-MS/MS method