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over a ramped temperature range of preferably 300–900 °C [ 1 ]. In this study, micro-scale combustion calorimetry (MCC) and thermogravimetric analysis coupled to Fourier transform infrared spectrometer (TG-FTIR) has been used to investigate the

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−1 stream of pure oxygen prior to entering a 900 °C combustion furnace. Thermogravimetry-Fourier transform infrared spectra The TG-FTIR instrument consists of TG analyzer (TGA-Q5000, TA Company, USA

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Journal of Thermal Analysis and Calorimetry
Authors: D. Wyrzykowski, E. Hebanowska, G. Nowak-Wiczk, M. Makowski, and L. Chmurzyński

,2,3-tricarboxylic acid. In our work the results of the TG-FTIR, TG-MS and DSC analyses of the three acids studied are presented. Experimental Materials All reagents: citric acid, C 6 H 8 O 7 , (ACS reagent, ≥99

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coated on the surface of cotton fabrics. The purpose of this research was to investigate the influence of the hybrid coating on thermal properties of cotton fabrics. The characteristics were evaluated through TG, TG-FTIR, and MCC experiments

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in a ceramic crucible up to 850 °C at a heating rate of 10 °C min −1 in dynamic air atmosphere ( v = 0.75 dm 3 h −1 ). For kinetic measurements, the heating rates: 5, 2.5 and 1.25 °C min −1 were applied. The TG–FTIR coupled measurements

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10 °C min −1 . 5–10 mg of the sample was examined under pure nitrogen at a flowing rate of 50 mL min −1 from 50 to 700 °C. TG coupled with Fourier transform infrared spectroscopy (TG-FTIR) consisted of a TGA/DSC 1 (Mettler/Toledo) coupled

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is so far to describe the thermal processes in details. So the aim of this study is to investigate thoroughly the thermal processes of enoxacin and ascertain the decomposition mechanism. For this purpose, the TG-FTIR technique, which can conduct

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Introduction In this article, our previous studies [ 1 – 4 ] on the thermal behavior of potentially active compounds are extended by applying the TG-FTIR technique over some new diazoamino-derivatives able to be used either as

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polymers. The aim of this study is to investigate the thermal decomposition of TFR and its polymer metal complexes using TG-FTIR-MS. Experimental Materials Thiourea, formaldehyde (37% aqueous solution), and

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halogenoacetates were analyzed as well as the presence of anions Cl − or Br − were also stated. The TG-FTIR coupled measurements have been carried out only for complexes II and IV using the Netzsch TG 209 apparatus coupled with Bruker FTIR spectrophotometer

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