XRPD pattern ( Fig. 8 c) shows an increase of the peak at 2ϑ = 22° and a decrease of the one at 14°, both relative to the spectrum of the sample annealed to 122 °C. Heating up to 160 °C produces a sample with smooth glassy surfaces broken by sharp holes
Authors:Máté Zsigmond Leskó, Richárd Zoltán Papp, Boglárka Anna Topa, Ferenc Kristály, Tamás Vigh, and Norbert Zajzon
carried out in the Institute of Mineralogy and Geology, University of Miskolc.
X-ray powder diffraction (XRPD) measurements were carried out using a Bruker D8 Advance diffractometer. The measurement parameters were the following: CuKα radiation, 40
Authors:Marco Júnio Peres-Filho, Marilisa Pedroso Nogueira Gaeti, Stela Ramirez de Oliveira, Ricardo Neves Marreto, and Eliana Martins Lima
there have been numerous reports on OLZ polymorphism, there are no literature reports regarding preformulation studies to support the design of solid dosage forms containing OLZ.
In this study, DSC, TG, and XRPD techniques were applied with the
Authors:Luciana Malpezzi, Elisabetta Maccaroni, Giordano Carcano, and Gianpiero Ventimiglia
diffraction pattern (XRPD) was collected at room temperature on an Ital-Structure θ/θ diffractometer, under the following condition: Ni-filtered Cu-Kα radiation (λ = 1.5418 Å); range 3° ≤ 2θ ≤ 40°; scan 0.04°; t = 2 s step −1 . The XRPD pattern was also
Authors:J. A. Stratis, M. Lalia-Kantouri, El. Charalambous, A. Charalambous, and N. Kantiranis
estimates of the abundance of the mineral phases were derived from the XRPD data, using the intensity of specific reflections, the density and the mass absorption coefficients of the elements for CuKα radiation for the minerals present. Corrections of the
Authors:A. Sykuła-Zając, E. Łodyga-Chruścińska, B. Pałecz, R. E. Dinnebier, U. J. Griesser, and V. Niederwanger
instrumental methods such as differential scanning calorimetry (DSC), X-ray powder diffraction (XRPD), and polarized light microscopy (PLM).
The present thermal and X-ray analysis was performed on the currently most popular racemic mixture of BupiHCl
Authors:Renu Chadha, Poonam Arora, Sushma Gupta, and Dharamvir Singh Jain
350 °C with a heating rate of 10 °C per min.
X-Ray powder diffraction (XRPD)
X-ray diffractometer (XPERT-PRO, PANalytical, Netherlands) with Cu as tube anode, voltage 40 kV, 35 mA, angular range 5, and fixed
Authors:Valentina Martena, Roberta Censi, Ela Hoti, Ledjan Malaj, and Piera Di Martino
corrected using the appropriate baselines recorded under identical conditions and converted to specific heat capacity curves.
X-ray powder diffractometry (XRPD) was used to check the amorphous state of the studied samples and to evaluate their
monochromators. The fluorescence maxima of compound 2 are gathered in Table 7 . The X-ray powder diffraction (XRPD) patterns were measured in reflection mode on an XPert PRO X-ray powder diffraction system equipped with a Bragg–Brentano PW 3050/65 high