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calorimetric analysis of various calcium sulfate phases during the gypsum hydration. Kuzel [ 5 ] presented comprehensive results on the hydration heats of pure α-calcium sulfates. Dantas et al. [ 11 ] used the temperature modulated differential scanning

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-isothermal temperature-modulated differential scanning calorimetry (TMDSC) for the separation of reversible and irreversible thermodynamic changes in glass transition and melting ranges of flexible macromolecules . Pure Appl Chem 81 : 1931 – 1952 10.1351/PAC-CON-08

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. 18. Gunaratne , LMWK , Shanks , RA . Thermal memory of poly(3-hydroxybutyrate) using temperature-modulated differential scanning calorimetry . J Polym Sci B Polym Phys 2006 44 : 70 – 78 10.1002/polb.20676

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heat capacity measurements by temperature-modulated differential scanning calorimetry . J Thermal Anal Calorim . 2010 ; 102 : 1135 – 1140 . 10.1007/s10973-010-0770-4 . 23. Hall , JA

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by temperature-modulated differential scanning calorimetry . J Therm Anal Calorim . 2010 ; 102 : 1135 – 1140 . 10.1007/s10973-010-0770-4 . 28. Zografi , G . States of water

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heat during the polymerisation process can be gathered out of these experiments. Therefore, the temperature modulated differential scanning calorimetry (TMDSC) technique was used to investigate characteristics of the specific heat during curing. This

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