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, collection procedure was repeated four times. The crude product was recrystallized from ethanol to afford 190.30 g (69.3% yield) of 4-nitrophthalimide as yellow crystals, mp 203 °C (DSC). ([ 6 ], 198 °C), decomposition onset 203 °C (TG): FTIR (ATR, cm −1

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Journal of Thermal Analysis and Calorimetry
Authors: Eveline De Robertis, Gabriela F. Moreira, Raigna A. Silva, and Carlos A. Achete

difficult to conclude anything based only in esters boiling points, for example, and there is no evidence of decomposition processes. Together with TG/FTIR data, some remarks can be done. These studies also tested biodiesels thermal behavior under

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Rare-earth based OLEDs

TG-FTIR thermal stability investigation of tetrakis beta-diketonates complexes

Journal of Thermal Analysis and Calorimetry
Authors: Kelly C. Teixeira, Gabriela F. Moreira, Welber G. Quirino, Cristiano Legnani, Raigna A. Silva, Marco Cremona, Hermi F. Brito, and Carlos A. Achete

resulting in the more stable tris-species. This does not happen for the Li[Eu(dbm) 4 ]·4H 2 O, which is thermally more stable, as the TG-FTIR measurement indicates. Conclusions The TG-FTIR results suggest that Li[Eu(dbm) 4

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Thermogravimetric analysis on gasification reactivity of Hailar lignite

Influence of inherent mineral matters and external ash

Journal of Thermal Analysis and Calorimetry
Authors: Ao Hou, Ze Wang, Wenli Song, and Weigang Lin

from Inner Mongolia of China is taken as the initial raw material, and its gasification characteristics is investigated by non-isothermal TG, FTIR, and X-ray diffraction (XRD) methods. The main objective of the study is to investigate the catalytic

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combustion properties were evaluated through microscale combustion calorimetry (MCC) experiment. In addition, TG, Real Time FTIR, and TG-FTIR were used to investigate the thermal degradation process of the materials. SEM and Raman diffusion measurements were

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Waste and fuels from waste

Part I. Analysis of thermal decomposition

Journal of Thermal Analysis and Calorimetry
Authors: Danuta Król and Sławomir Poskrobko

. Galvagno , S , Casu , S , Martino , M E Di Palma Portofino , S 2007 Thermal and kinetic study of tyre waste pyrolysis via TG–FTIR–MS analysis . J Therm Anal Calorim 88 2 507 – 514 10.1007/s10973-006-8409-1 . 9

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Co-firing of biomass with coals

Part 1. Thermogravimetric kinetic analysis of combustion of fir (abies bornmulleriana) wood

Journal of Thermal Analysis and Calorimetry
Authors: Ahu Gümrah Dumanli, Sinem Taş, and Yuda Yürüm

heat transfer limitations, was thinly distributed in the crucible in the experiments. The experiments were replicated at least twice to determine their reproducibility, which was found to be satisfactory. The TG–FTIR runs were carried out in a

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, Wójtowicz , MA . TG-FTIR analysis of biomass pyrolysis . Fuel . 2001 ; 80 : 12 1765 – 1786 . 10.1016/S0016-2361(01)00061-8 . 4. Yang , H , Yan , R , Chin , T , Liang , DT , Chen

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Journal of Thermal Analysis and Calorimetry
Authors: Rosely dos Reis Orsini, Elder Moscardini Filho, Lucildes Pita Mercuri, Jivaldo do Rosário Matos, and Fátima Maria Sequeira de Carvalho

. Souza , BS , Moreira , APD , Teixeira , AMRF . TG-FTIR coupling to monitor the pyrolysis products from agricultural residues . J Therm Anal Calorim . 2009 ; 97 : 637 – 642 . 10.1007/s10973-009-0367-y . 20

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loss and apparent activation energy Oxidation model of cellulose/CuO mixtures An oxidation model of cellulose/CuO mixtures was proposed by DSC, TG, FT-IR, and kinetic analyses results

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