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highly aggressive reagents in a minimum amount of solvent (AlCl 3 in propionyl chloride and neat ICl), in combination with high-temperature operation, allowed the completion of the whole reaction sequence with unprecedented speed in an overall yield of

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after aggressive milling. Small, separated particles are ideal for reinforcing a polymer matrix and improvement their thermal and barrier properties [ 1 , 2 ]. With the rapid development of nanotechnologies and nanomaterials since 1990s, the

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