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h in the case of the Aa and Ac glasses were applied. For the purpose of learning the thermal properties of the glasses, their thermal analysis was carried out. DSC measurements were taken using the STA 449 Jupiter F3 apparatus of the Netzsch

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the course of their synthesis process itself. Thermal analysis is used [ 12 – 17 ] for the TG monitoring of the synthesis of MCM-41 mesoporous materials being obtained from silicon sources, such as regular silica-gel or colloidal fumed silica, which

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. Biedunkiewicz , A , Gabriel , U , Figiel , P , Grzesiak , D 2010 Application of thermal analysis in nanotechnology, carbonization and purification of nc-TiC x in argon atmosphere . J Therm Anal Calorim 101 2 701 – 706 10.1007/s10973

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Journal of Thermal Analysis and Calorimetry
Authors: Wiesława Ferenc, Beata Cristóvão, Jan Sarzyński, and Paweł Sadowski

charge density around atoms [ 23 ]. Thermal analysis The thermal properties of the 4-methoxycinnamates of Mn(II), Co(II), Ni(II), Cu(II), Cd(II), Nd(III) and Gd(III) were investigated by means of TG, DTG and DSC

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Journal of Thermal Analysis and Calorimetry
Authors: G. Janowska, A. Kucharska-Jastrzabek, W. M. Rzymski, and A. Pajak

machine, model 1435, cooperating with a properly programmed computer. Dumbbells with a measurement section width of 4 mm were used to determine tensile strength ( TS b ) and elongation at break ( E b ) [ 16 ]. The thermal analysis of cross

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(Mettler Toledo AG, Giessen, Germany) equipped with an automatic refrigerated cooling accessory (RCS) and modulated capability, an auto-sampler tray (TSO 801R0 Mettler Toledo) and a thermal analysis data system. Nitrogen was used as the purge gas at a flow

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transition detected by the thermal analysis (ca. 464 and 480 K in Fig. 2 a), a PXRD analysis at variable temperature was carried out ( Fig. 7 ). Fig. 7 Variable temperature PXRD patterns heating at a rate of 0

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. Vyazovkin , S . et al. 2011 ICTAC kinetics committee recommendations for performing kinetic computations on thermal analysis data . Thermochim Acta 520 : 1 – 19 10.1016/j.tca.2011.03.034 . 2

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.02.043 . 8. Bourgeois , J , Pierson , L , Nicolas , J . Application of thermal analysis to the study of lipidic prodrug incorporation into nanocarriers . J Therm Anal Calorim . 2009 ; 98 : 65 – 71 . 10.1007/s10973

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, all the samples were examined by differential thermal analysis DTA/TG and by X-ray diffraction method to determine their composition. Table 1 The composition of the initial mixtures and the conditions of

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