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Acta Chromatographica
Authors:
Aixia Han
,
Guanyang Lin
,
Jinzhang Cai
,
Qing Wu
,
Peiwu Geng
,
Jianshe Ma
,
Xianqin Wang
, and
Chongliang Lin

– ∞ ) ng/mL*h 324.1 ± 54.2 176.1 ± 19.7 b MRT (0– t ) h 5.0 ± 0.8 3.1 ± 0.2 b

Open access

.00 550 °C (12 h) 50.00 MoO 3 , + 50.00 In 2 (MoO 4 ) 3 6 75.00 25.00 Stage II: In 2 (MoO 4 ) 3 a

Open access

] − 412 70 Oxedhyperforin H 50.56 554 553 [M − H] − 484

Open access

found (ng mL −1 , mean ± SD) Precision (%RSD) Accuracy (%) Bench top (up to 9 h) 5.0  4.7 ± 0

Open access
Acta Chromatographica
Authors:
Jinzhao Yang
,
Huamin Liu
,
Yuan Cai
,
Yazhen Wu
,
Xiaoxin Xu
,
Xianqin Wang
, and
Chongliang Lin

chromatography separation, limonin (C 26 H 30 O 8 ) and β-sitosterol (C 29 H 50 O) were extracted from the seeds and pulp of Citrus suavissima Hort. ex Tanaka , respectively [ 5 ]. Their structures were identified by spectral analysis ( 1 H NMR, 13 C NMR, DEPT

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.6 ± 1.6 MRT (0−∞) h 7.2 ± 6.6 6.1 ± 2.5 t 1/2 z h 5.0 ± 3.0 3.5 ± 1.8 V z L/kg 35.9 ± 26.9 85.8 ± 23.6 CLz L/h/kg 6.0 ± 2.1 18.8 ± 6.9 C max ng/mL 90.2 ± 8.2 81.0 ± 12.4 Bioavailability 37.5% Conclusion In this study, a simple and fast UPLC-MS/MS method

Open access