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The absolute values of the Debye-Waller factor for high-spin Fe/pyrrdtc/3 and low-spin Fe/pyroldtc/3 iron/III/ complexes /pyrrdtc-pyrrolidyl-N-carbodithioato, pyroldtc-pyrrole-N-carbodithioato/ were determined at room temperature. The obtained values of mean square displacement <x2> are in very good agreement with those determined by X-ray diffraction methods.

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