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was determined as C 13 H 12 N 3 OS 2 ClNi. The second decomposition stage at which the C 11 H 12 NOCl left out this intermediate product was observed in the temperature range of 547–708 K. The mass loss of this elimination was about 33.50% (Calc.:35
. Pharm. Bull. 2013 , 61 , 1269 . 10.1248/cpb.c13-00547 9. Zhang , Y. ; Yang , B. ; Gan , J. ; Liu , C. G. ; Shu , X. ; Shu , J. N. Atmos
porosity and other geometric factors [ 10 ]. It was found to be limited by diffusion even at fairly low temperatures (~600 °C) [ 13 ]. These effects are not expected to be significant for the small samples of micrometer-sized powders with narrow particle
.4 (C-5′), δ C 10.6 (C-6′), δ C 23.3 (C-7′), and δ C 13.7 (C-8′), on the basis of its spectral data compound 4 was identified as di-(2-ethylhexyl) phthalate [ 29 , 30 ]. Compound 5 was obtained as fine powder ( R f upon PC in 15% AcOH
-12), 113.8 (C-13), and 133.3 (C-14) ppm. The anomeric proton assigned at δ 5.01 ppm (d, J = 5.4 Hz) through its one-bond correlation in Heteronuclear Single Quantum Coherence (HSQC) with its own anomeric carbon signal at δ 100.5 ppm was an
Thermochemical production of hydrogen
Synthesis, characterization, and decomposition of copper oxychloride
°C (13.2 mg argon, 15.8 mg air) held for 12 h and then heated to 800 °C (air and argon flow rate: 50 mL/min) and in air, the mass is constant after 3 h at 530 °C and the run was stopped there. Runs in air are represented by dashed lines while runs
Crystal structures and thermal properties of some rare earth alkoxides with tertiary alcohols
Possible precursors for atomic layer deposition of rare earth oxides
.17(3) c = 23.625(5) c = 12.363(6) γ = 93.28(3) c = 12.156(2) c = 13
Magnesium sulphate complexes with hexamethylenetetramine and 1,10-phenanthroline
Thermal, structural and spectroscopic properties
dimensions (Å, °): a = 12.0010(10), b = 10.0779(7), c = 13.8536(10), α = 90.00, β = 113.459(8), γ = 90.00; volume (Å 3 ): 1537.0(2); reflections collected/unique: 15987/2735 (R (int) = 0.0512); data/restraints/parameters: 2735/0/214; GooF: 1.157; final
