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A calorimetric method is proposed to evaluate the catalytic activity of a solid catalyst with respect to the exothermic oxidation of Volatile Organic Compounds (VOC).

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The enthalpy of the reduction of UO2F2 with hydrogen was obtained from quantitative DTA measurements with a linear heating rate and under isothermal conditions, and the thermodynamic data on UO2F, formed as a stable intermediate in the reduction of UO2F2 to UO2, are also presented. The advantages of isothermal DTA in the reduction of U3O8 to UO2 could be demonstrated.

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