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-oxidation stability of the resin and buckypaper was evaluated by TGA considering that the surface temperature of materials in cone calorimeter at 50 kW/m 2 external heat fluxes can reach around 500 °C [ 13 ]. Figure 5 shows the TGA curves in air. The onset
. Fig. 3 FT-IR spectra of Cd 2+ /TREN solution ( R c = 1–3, = 50 mM) and of free TREN ( bold line ) When the stability of the 1:1 complex formed is compared with available data in
– – – – Δ T m /°C 13–80 – – – – Δ T 0 /°C 193–358 191–344 174
carbonized material is then subject to a gasification process with a steam-nitrogen mixture [ 12 ]. The temperature is varied between 600 and 900 °C [ 13 ] and the residence times between 1 and 10 h, with the aim of studying the effect during the activation
, BD , Kim , YS , Singh , AP , Lim , KP . Reactivity, chemical structure, and molecular mobility of urea-formaldehyde adhesives synthesized under different conditions using FTIR and solid-state C-13 CP/MAS NMR Spectroscopy . J Appl Polym Sci
2 during the thermal analysis is already known. In the case of this oxide partial oxygen loss was detected by TG–DTA measuring which corresponds with one endothermic effect at the temperature 1449 °C [ 13 ]. By TG curve the mass lost at the
. 12. Tabero , P , Filipek , E 2004 Synthesis and properties of a solid solution formed in the CrVMoO 7 -AlVMoO 7 system . J Therm Anal Calorim 77 : 183 – 191 10.1023/B:JTAN.0000033202.46419.2c
obtained from the molar heat capacity [ 15 , 16 ]. In this paper, the phase change properties and the thermal stability of an N - tert -butyloxycarbonylated organic synthesis intermediate, ( S )- tert -butyl 1-phenylethylcarbamate (Scheme 1 , C 13 H 19
, and shampoo samples (50 μL), and then the mixture were vortex-mixed for 1 min. After centrifugation at 4 °C, 13,000 rpm for 5 min, the chloroform layers (50 μL) were diluted with MeOH (50 μL). The processed samples (5 μL) were analyzed by LC