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Acta Chromatographica
Authors: Qinghua Weng, Lianguo Chen, Luxin Ye, Xiaojie Lu, Zheng Yu, Congcong Wen, Yichuan Chen, and Gang Huang

/mL for evaluating accuracy, precision, and stability. All the solutions were stored at 4 °C until processed. Preparation of Plasma Samples Licochalcone A and IS were simultaneously extracted from the plasma specimens

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, linearity, limit of detection (LOD), limit of quantification (LOQ), accuracy, precision and robustness of drug in plasma were assessed. Selectivity The selectivity of developed method was performed by evaluating blank as well as CAP samples The RT was

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Acta Chromatographica
Authors: Andreea Silvia Neamţu, Andrei Biţă, Ion Romulus Scorei, Gabriela Rău, Ludovic Everard Bejenaru, Cornelia Bejenaru, Otilia-Constantina Rogoveanu, Carmen Nicoleta Oancea, Antonia Radu, Cătălina Gabriela Pisoschi, Johny Neamţu, and George Dan Mogoşanu

0.2 mL/min. The nebulizing and drying gas used was nitrogen. Method Validation The proposed method was validated by specificity, linearity range, accuracy, precision, limit of detection (LOD), limit of

Open access

samples for the evaluation of intra- and inter-batch precision and accuracy, matrix effect, and stability were 1.5, 30, and 750 ng/mL for remimazolam and 60, 1200, and 30,000 ng/mL for M1, respectively. IS working solutions (100 ng/mL for remimazolam and

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Acta Chromatographica
Authors: Aixia Han, Guanyang Lin, Jinzhang Cai, Qing Wu, Peiwu Geng, Jianshe Ma, Xianqin Wang, and Chongliang Lin

Administration (FDA) [ 24 ]. The validation work included selectivity, matrix effect, linearity, precision, accuracy, recovery, and stability. Selectivity of the UPLC–MS/MS method was evaluated by detecting six lots of blank plasma, blank plasma spiked

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Acta Chromatographica
Authors: Yun Wang, Jianhong Chen, Yutian Li, Puling Li, Javed Iqbal, Ying Chen, Yinlian Ma, and Cun Zhang

Method Validation The linear relationship, limit of detection (LOD), limit of quantification (LOQ), recovery, precision, and relative standard deviation (RSD) are shown in Tables 2 , 3 , and 4 to evaluate the quality of this method. The

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Acta Chromatographica
Authors: Yongxi Jin, Yuyan Chen, Jiawen Liu, Xi Bao, Yinghao Zhi, Congcong Wen, and Wenzong Zhu

guidelines [ 14 – 19 ]. Validation projects included selectivity, matrix effects, linearity, precision, accuracy, recovery, and stability [ 20 – 24 ]. The selectivity of the method was evaluated by analyzing 6 lots of different sources of blank

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Acta Chromatographica
Authors: Lenche Velkoska-Markovska, Mirjana S. Jankulovska, Biljana Petanovska-Ilievska, and Kristijan Hristovski

. Method Validation Validation of the method for determination of chlorogenic acid in green coffee was performed testing following parameters: linearity, specificity, selectivity, precision, accuracy, limit of detection (LOD), and limit of

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Acta Chromatographica
Authors: Xi Bao, Bingge Huang, Yiting Mao, Zhiguang Zhang, Yunfang Zhou, Congcong Wen, and Quan Zhou

verification method was established in accordance with the US Food and Drug Administration (FDA) bioanalytical method validation guidelines. Validation projects include selectivity, matrix effects, linearity, precision, accuracy, recovery, and stability

Open access

/mL. All solutions were stored at 4 °C and brought to room temperature before use. Calibration standards and quality control (QC) samples used to estimate precision and accuracy of the method were prepared from two separate sets of solutions in

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