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(Siglufjordur, Iceland). Dough mixer “MONO” (Swansea, UK) was used to make dough at two stirring rates during 10 min. The dough was allowed to proof for 25–30 min at 38 °C and relative humidity 72% and cut to pieces with weight 65 g. The rolls were baked in

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Journal of Thermal Analysis and Calorimetry
Authors: Edilene P. Lavor, Fátima Duarte Freire, Cícero Flávio S. Aragão, Fernanda N. Raffin, and Túlio Flávio A. de Lima e Moura

–solid phase transitions upon heating [ 19 ]. Studies of interaction performed by Bhutan et al. [ 27 ] and Singh et al. [ 6 ] reported that the mixture between INH and ETA becomes liquid under accelerated conditions of temperature and relative humidity

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was in average temperature ranged between 20 and 22 °C and the relative humidity (RH) ranged between 65 and 67%. Method of evaluation Flammability test The vertical flame spread test method by

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at a rate of 5 °C per minute. TG data were collected every 4 s. During analyses, the furnace and the sample were purged with the constant air stream of 76% relative humidity at 25 °C and flow rate of 200 ml min −1 . To ensure comparable

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Guidelines for the Care and Use of Laboratory Animals. The rats were acclimated in the laboratory for 1 week prior to the experiments, housed in separate cages at a temperature of 23 ± 2 °C with a 12 h light–dark cycle and a relative humidity of 50%, and with

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(INSTRON model 1405). Experiments were carried out at constant cross-head speed of 5 mm min −1 with relative humidity of 65% at 20 °C. Before subjecting the samples to analysis, dumbbell shaped samples of uniform width and thickness were made and analyzed

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] mass ratio of 0.5:1:3. After curing at 20 ± 1 °C and 90% relative humidity (RH) for 24 h, the specimens were demoulded and cured in lime-saturated water at 20 ± 1 °C, followed by strength tests according to EN 196-1 [ 15 ]. Figure

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.5. Pharmacokinetic Analysis Twelve male SD rats (200 ± 20 g), which were 7–8 weeks old, were provided by the Experimental Animal Center of Wenzhou Medical University. Rats were placed at a relative humidity of 55 ± 10% and a temperature of 22 ± 2 °C. The

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Male Sprague–Dawley (SD) rats (210–250 g) were supplied by Samtako (Incheon, Korea). Prior to carrying out experiments, the rats were housed at a temperature of 22 ± 2 °C and relative humidity of 50 ± 10%, under a 12-h light–dark cycle for 7 days, with

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using a Fire Testing Technology cone calorimeter (Fire Testing Technology Ltd., UK). The dimensions of the samples were 100 mm × 100 mm and the thicknesses are shown in Table 1 . The samples were conditioned to equilibrium at 55% relative humidity (RH

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