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Salts [XanH+]2[MCl

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Journal of Thermal Analysis and Calorimetry
Authors: L. E. Garcia-Megias, E. Colacio-Rodriguez, A. Garcia-Rodriguez, J. Ruiz-Sanchez, and J. M. Salas-Peregrin

The thermal behaviour of 6-amino-5-formyluracil (HFU), 6-amino-1-methyl-5-formyluracil (1-MFU), 6-amino-3-methyl-5-formyluracil (3-HFU) and 6-amino-1,3-dimethyl-5-formyluracil (HDFU) is described. Only HDFU is shown to contain crystallization water. Dehydration and fusion enthalpy values have been calculated from the DSC curves. Likewise, the thermal behaviour of new complexes obtained by reaction between the above pyrimidine derivatives and Ni(II), Cu(II) and Pd(II) ions is reported.

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Tetrachloroaurates of 8-ethyl-, 8-isopropyl-, 8-propyl- and 8-pentyltheophylline were synthesized and studied by1H-NMR, TG and DSC techniques. The metal is not coordinated to the 8-alkyltheophylline derivatives and forms a salt-like structure.

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