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Journal of Thermal Analysis and Calorimetry
Authors: Viorel Sasca, Elena Mosoarca, Livia Avram, Ramona Tudose, and Otilia Costisor

Abstract  

The thermal decomposition of Mannich base N,N′-tetra(4-antipyrylmethyl)-1,2-diaminoethane (TAMEN), and its Ni(II), binuclear complex, Ni2(TAMEN)Cl4, in air and in nitrogen atmosphere, were investigated. X-ray powder diffractometry, infrared spectroscopy and simultaneous thermogravimetry-differential thermal analysis (TG-DTA), have been used to characterize and to study the thermal behavior of these compounds. The results provided information concerning the stoichiometry, crystallinity, thermal stability and decomposition mechanism of the compound.

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Journal of Thermal Analysis and Calorimetry
Authors: Elena Mosoarca, Sasca Viorel, Livia Avram, Ramona Tudose, and Otilia Costisor

Abstract  

The thermal decomposition in air and in nitrogen atmosphere of binuclear complex compounds of Cu(II) and Co(II) containing the Mannich base N,N′-tetra(4-antipyrylmethyl)-1,2 diaminoethane (TAMEN) as a ligand, Cu2(TAMEN)Cl4 and Co2(TAMEN)Cl4, were investigated. X-ray powder diffractometry, infrared spectroscopy and simultaneous thermogravimetry-differential thermal analysis (TG-DTA), have been used to characterize and to study the thermal behavior of these compounds. The results provided information concerning the stoichiometry, crystallinity, thermal stability and decomposition mechanism of the compounds.

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