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Journal of Thermal Analysis and Calorimetry
Authors:
M. Lalia-Kantouri
,
G. A. Katsoulos
, and
F. D. Vakoulis
Thermal studies by TG and DTG on some homobinuclear dihalide-bridged iron(III) complexes of the general type [Fe(S2CNR2)2X]2(μ}-X′ 2) were carried out in air and nitrogen atmospheres. The apparent activation energies were determined by graphical methods and the TIN temperatures were calculated from the TG profiles. Finally, a possible mechanism of the decomposition is suggested on the basis of the pyrolysis and mass spectral data.
Journal of Thermal Analysis and Calorimetry
Authors:
G. A. Katsoulos
,
M. Lalia-Kantouri
, and
F. D. Vakoulis
Mass spectral and thermal studies by TG and DTG of some iron(III) binuclear complexes of the general type Fe2(R2dtc)2(tds∮)X2X/′ have been carried out to determine their modes of decomposition. Fragmentation patterns are given and possible mechanisms are discussed.
