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In thermal analysis polyethylenes can be characterized by their melting temperature. With the polyethylene mixtures studied, we obtained the best results during solidification. Crystallization temperature decreased in the order: high density PE, low density PE linear, radical low density PE.

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Journal of Thermal Analysis and Calorimetry
Authors:
L. El Watik
,
P. Antonetti
,
Y. Claire
,
H. Zineddine
,
J. Kaloustian
,
C. Rossi
, and
A. Perichaud

Abstract  

The authors studied the ignifugation and the kinetic of thermal degradation of the Styrene-Butadiene copolymer with an intumescent system Ammonium polyphosphate-Pentaerythrinol-Melamine. For that, they used the thermogravimetric and oxygen index techniques. The best formulation of intumescent system which can give the optimum results is proposed.

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Abstract  

The oxidation of pure and recycled polyethylene samples was studied by thermal analysis (DTA-TG-DSC): presence of two exothermic peaks and mass loss. The thermo-oxidation products, containing C-O and C=O links, were identified by IR spectrometry and GC-MS spectrometry. The oxidation is easier from low to high density polyethylene.

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Journal of Thermal Analysis and Calorimetry
Authors:
L. El Watik
,
Y. Claire
,
H. Zineddine
,
C. Rossi
,
J. Kaloustian
,
M. Sergent
, and
A. Périchaud

Abstract  

The study of the thermal degradation of the fireproof polystyrene—butadiene copolymer by an intumescent system: ammonium polyphosphate (APP)—pentaerythritol (PER)—talc (TAL), was done through an experimental process. Thermogravimetry under air sweeping was used. We observed for the degradation rate of the mixture with fireproofing agents, in the field of 20 to 50% mass loss, a better linear increasing when this mixture contains more TAL and the ratio APP/PER is smaller.

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