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The theory of errors of three variants of sub- and super equivalence method is given and errors for typical cases are tabulated. The principles of the variants are described. Recommendations are offered for a rational choice of a variant to be used and for that of the parameter . For the calculations the assumption is used that the analysis is based on the solvent-extraction equilibrium+ A+BABorg.

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). Rational choice of the conditions for prior heat treatment of the samples, to achieve thermal analysis, allows the highlighting of the exothermic processes that accompany the formation of CA 6 . The information provided by thermal analysis are confirmed by

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