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Journal of Thermal Analysis and Calorimetry
Authors: Yu. Trach, V. Sydorchuk, O. Makota, S. Khalameida, R. Leboda, J. Skubiszewska-Zięba, and V. Zazhigalov

not detected by means of used methods of investigations. The increase of specific surface area of milled samples (C3, C4) confirms the latter suggestion. UV–Vis spectroscopy study It is well known that the results

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Journal of Thermal Analysis and Calorimetry
Authors: V. Sydorchuk, O. Makota, S. Khalameida, L. Bulgakova, J. Skubiszewska-Zięba, R. Leboda, and V. Zazhigalov

spectroscopy More detailed information about structure of deposited phases was obtained with the help UV–Vis spectroscopy that get a deeper insight on the state of the vanadia and molybdena at support surface [ 19 ]. It is known that UV–Vis absorption

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Journal of Thermal Analysis and Calorimetry
Authors: P. S. Epaminondas, K. L. G. V. Araújo, J. A. Nascimento, M. C. D. Silva, R. Rosenhaim, L. E. B. Soledade, N. Queiroz, A. L. Souza, I. M. G. Santos, and A. G. Souza

function of the overall peak area. The physico-chemical properties were measured according to the methods described by AOCS [ 8 ]. The oil samples were also characterized by UV–Vis spectroscopy using a Shimadzu UV-2550 spectrophotometer at the 200

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Journal of Thermal Analysis and Calorimetry
Authors: J. Maul, A. S. Brito, A. L. M. de Oliveira, S. J. G. Lima, M. A. M. A. Maurera, D. Keyson, A. G. Souza, and I. M. G. Santos

to form Cu 2 O at around 1039–1043 °C. Wang et al. [ 8 ] reported the same synthesis using copper acetate in ethanolic solution with NaOH and showed by using UV–Vis spectroscopy that absorption peak of CuO is located at about 340 nm and no presenting

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Reaction Kinetics, Mechanisms and Catalysis
Authors: Mohammad Saleh Ghodrati, Mohammad Haghighi, Jafar Sadegh Soltan Mohamdzadeh, Behzad Pourabas, and Ehsan Pipelzadeh

media at 25 °C. Samples were taken at 15 min intervals from the reaction media and filtered using a 0.45 μm filter to form a clear solution. Further investigation of photocatalytic performance was conducted using a Philips UV–vis spectroscopy, indicating

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Journal of Thermal Analysis and Calorimetry
Authors: F. T. G. Vieira, A. L. M. Oliveira, D. S. Melo, S. J. G. Lima, E. Longo, A. S. Maia, A. G. Souza, and I. M. G. Santos

are difficult to eliminate after formation. Elimination of the organic material was evaluated by thermal analysis (TG/DTA) and infrared spectroscopy. X-ray diffraction was used to evaluate the crystallization, while UV–vis spectroscopy permitted to

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radiation wavelength, k = 0.90 and 2θ is the Bragg angle [ 14 ]. UV–Vis spectroscopy was also utilized to measure the optical transmittance of the produced films using a Varian Cary 500 Scan spectrophotometer. To evaluate the catalytic activity

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DTA curves ( a ) TiO 2 , ( b ) CdSe, ( c ) TiO 2 + CdSe, ( d ) TiO 2 + CdSe + linker UV–Vis spectroscopy Figure 5 shows the normalized UV–Vis absorption of TiO 2

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Journal of Thermal Analysis and Calorimetry
Authors: D. Melo, R. M. M. Marinho, F. T. G. Vieira, S. J. G. Lima, E. Longo, A. G. Souza, A. S. Maia, and I. M. G. Santos

and could be confirmed by UV vis spectroscopy that showed higher amounts of Cu(I) for samples with higher copper amount and higher heat treatment temperatures. The authors acknowledge Coordination of Improvement of Higher

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Abstract  

Differential scanning microcalorimetry (DSC) and UV–VIS absorption spectroscopy were used to obtain the characteristics of blood serum from newborn rat’ after maternal treatment with cyclophosphamide in comparison with control. The obtained DSC curves reveal a complex endothermic peak due to the unfolding process of various serum proteins. Thermal profiles and absorption spectra of blood serum are sensitive to the age of newborns as well as to effect of maternal administration of cyclophosphamide. The most significant disturbances in serum proteome were observed for 14-day old newborns. The thermodynamic parameters: enthalpy change (∆H), the normalized first moment (M1) of the thermal transition with respect to the temperature axis and the ratio of C p ex at 70 and 60 °C describing denaturation contributions of globulin forms in respect to unliganded albumin with haptoglobin was estimated. Moreover, the second derivative spectroscopy in the UV region was used to resolve the complex protein spectrum. The differences in blood serum detected by DSC and UV–VIS confirm a potential usefulness of these methods for diagnostic and monitoring changes with age as well as the pathological state of blood serum.

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