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Preparation of microspherical granules from aerosilogels

The way of spray drying in overheated water steam

Journal of Thermal Analysis and Calorimetry
Authors: Jadwiga Skubiszewska-Zięba and V. Sydorchuk

Abstract  

The influence of the conditions of aerosil dispersion spray drying process in the medium of overheated water steam on the formation of microspheric granules and their porous structure was studied. Water and ammonium solutions as aerosil particles dispersing agents and water steam and air as heat carriers were used. It was stated that the effects of spray drying depend on the kind of dispersing medium and on the conditions of atmosphere and temperature at which drying and forming of aerosilogel granules takes place.

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Journal of Thermal Analysis and Calorimetry
Authors: Yu. Trach, V. Sydorchuk, O. Makota, S. Khalameida, R. Leboda, J. Skubiszewska-Zięba, and V. Zazhigalov

aerosilogel prepared in the same conditions using water. In this case, last two parameters ( V s and V Σ ) are equal, which indicates homogeneous mesoporous structure of sample C0; it can be seen from Table 1 and in Fig. 5 (isotherms 1 and 2

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Journal of Thermal Analysis and Calorimetry
Authors: V. Sydorchuk, S. Khalameida, J. Skubiszewska-Zięba, and R. Leboda

nitrogen adsorption–desorption and pore size distribution (insert) for initial aerosilogel ( 1 ), and compositions based on A380 containing 20% w/w AMP: initial ( 2 ), and milled in water at 200 rpm ( 3 ), 400 rpm ( 4

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