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The study of the dehydration/rehydration of ammonium tris-oxalato aluminate(III) (NH4)3Al(C2O4)3⋅3H2O in flowing dinitrogen saturated with water vapor at room temperature, using thermogravimetric analysis and X-ray diffraction techniques, allowed the determination of the temperature stability domains of (NH4)3Al(C2O4)3⋅3H2O, (NH4)3Al(C2O4)3⋅2H2O and the anhydrous salt. The X-ray powder diffraction profiles are reported for each of the three phases.

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