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The formation of benzynes derivatives from ortho-trimethylsilyl triflates using tetra-n-butylammonium fluoride (TBAF) as the benzyne-forming trigger was achieved in a straightforward flow reactor at room temperature. These benzynes were immediately trapped in Diels—Alder reactions to deliver the desired cycloadducts.

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carbide microreactor” S. G. Newman, L. Gu, C. Lesniak, G. Victor, F. Meschke, L. Abahmane, K. F. Jensen* Green Chemistry 2014 , 16 , 176–180 “Three-component coupling based on flash chemistry. Carbolithiation of benzyne with

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