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Abstract  

TG, DTA and DSC curves of Cd2[Ti2(O2)2O(OH)6]·H2O were recorded and used to determine the isothermal conditions suitable for obtaining the intermediate samples corresponding to the phases observed during the thermal decomposition. The samples were identified by quantitative analysis, IR spectroscopy and X-ray analysis. The experimental results were used to propose a mechanism of thermal decomposition of the investigated compound to CdTiO3. The optimum conditions were also determined for obtaining CdTiO3 with well-defined crystallinity.

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