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Jasenka Živko-BabićUniversity of Zagreb Department of Prosthodontics, School of Dental Medicine 10000 Zagreb Gundulićeva 5 Croatia

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Marica Medić-ŠarićUniversity of Zagreb Department of Pharmaceutical Chemistry, Faculty of Pharmacy and Biochemistry 10000 Zagreb A. Kovačića 1 Croatia

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Ana MornarUniversity of Zagreb Department of Pharmaceutical Chemistry, Faculty of Pharmacy and Biochemistry 10000 Zagreb A. Kovačića 1 Croatia

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Marko JakovacUniversity of Zagreb Department of Prosthodontics, School of Dental Medicine 10000 Zagreb Gundulićeva 5 Croatia

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Ivona JaspricaUniversity of Zagreb Department of Pharmaceutical Chemistry, Faculty of Pharmacy and Biochemistry 10000 Zagreb A. Kovačića 1 Croatia

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Srećko TurinaUniversity of Zagreb Department of Pharmaceutical Chemistry, Faculty of Pharmacy and Biochemistry 10000 Zagreb A. Kovačića 1 Croatia

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Titanium as the pure metal or as commercial titanium alloys has been widely used in dentistry. To determine the composition of incorporated reconstructions there is a need for non-destructive sampling and identification of unknown or suspect elements. This paper reports an analytical procedure for detection of titanium. The method involves anodic sampling, and separation and identification of titanium by thin-layer chromatography (TLC) on precoated cellulose layers. Two thin plates and one cast of elemental titanium and one dental alloy containing titanium were analyzed. Chromatograms of samples were developed with a mixture of iso -amyl alcohol, acetonitrile and hydrochloric acid as mobile phase. Excellent detection and identification of titanium as a pink spot was achieved after spraying with a saturated ethanolic solution of alizarin and exposure to NH 3 vapor.

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Journal of Planar Chromatography - Modern TLC
Language English
Size A4
Year of
Foundation
1988
Volumes
per Year
1
Issues
per Year
6
Founder Akadémiai Kiadó
Founder's
Address
H-1117 Budapest, Hungary 1516 Budapest, PO Box 245.
Publisher Akadémiai Kiadó
Springer Nature Switzerland AG
Publisher's
Address
H-1117 Budapest, Hungary 1516 Budapest, PO Box 245.
CH-6330 Cham, Switzerland Gewerbestrasse 11.
Responsible
Publisher
Chief Executive Officer, Akadémiai Kiadó
ISSN 0933-4173 (Print)
ISSN 1789-0993 (Online)

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