Author:
Authors:
,
,
,
,
,
,
, and
M. Ganesh
M. Ganesh
Department of Pharmaceutical Analysis, Nandha College of Pharmacy Koorapalayam Pirivu, Erode 638052, Tamil Nadu, India
Search for other papers by M. Ganesh in
Current site
Google Scholar
PubMed
Search for other papers by M. Ganesh in
Current site
Google Scholar
PubMed
B. Thangabalan
B. Thangabalan
Department of Pharmaceutical Analysis, Nandha College of Pharmacy Koorapalayam Pirivu, Erode 638052, Tamil Nadu, India
Search for other papers by B. Thangabalan in
Current site
Google Scholar
PubMed
Search for other papers by B. Thangabalan in
Current site
Google Scholar
PubMed
R. Patil
R. Patil
Department of Pharmaceutical Analysis, Nandha College of Pharmacy Koorapalayam Pirivu, Erode 638052, Tamil Nadu, India
Search for other papers by R. Patil in
Current site
Google Scholar
PubMed
Search for other papers by R. Patil in
Current site
Google Scholar
PubMed
D. Thakur
D. Thakur
Department of Pharmaceutical Analysis, Nandha College of Pharmacy Koorapalayam Pirivu, Erode 638052, Tamil Nadu, India
Search for other papers by D. Thakur in
Current site
Google Scholar
PubMed
Search for other papers by D. Thakur in
Current site
Google Scholar
PubMed
A. Kumar Kumar
A. Kumar Kumar
Department of Pharmaceutical Analysis, Nandha College of Pharmacy Koorapalayam Pirivu, Erode 638052, Tamil Nadu, India
Search for other papers by A. Kumar Kumar in
Current site
Google Scholar
PubMed
Search for other papers by A. Kumar Kumar in
Current site
Google Scholar
PubMed
M. Vinoba
M. Vinoba
Department of Chemical Engineering, Alagappa College of Technology, Anna University, Guindy, Chennai, 600 025, Tamil Nadu, India
Search for other papers by M. Vinoba in
Current site
Google Scholar
PubMed
Search for other papers by M. Vinoba in
Current site
Google Scholar
PubMed
S. Ganguly
S. Ganguly
Department of Pharmaceutical Sciences, Birla Institute of Technology, Mesra, Ranchi, Jharkhand, India
Search for other papers by S. Ganguly in
Current site
Google Scholar
PubMed
Search for other papers by S. Ganguly in
Current site
Google Scholar
PubMed
T. Sivakumar
T. Sivakumar
Department of Pharmaceutical Analysis, Nandha College of Pharmacy Koorapalayam Pirivu, Erode 638052, Tamil Nadu, India
Search for other papers by T. Sivakumar in
Current site
Google Scholar
PubMed
Search for other papers by T. Sivakumar in
Current site
Google Scholar
PubMed
Summary
A rapid, simple and validated reversed-phase high-performance liquid chromatographic method has been developed for analysis of oxaprozin in pharmaceutical dosage forms. Oxaprozin was separated on an ODS analytical column with a 45:55 (v/v) mixture of acetonitrile and triethanolamine solution (5 mm, pH 3.5 ± 0.05, adjusted by addition of 85% phosphoric acid) as mobile phase at a flow rate of 2.0 mL min–1. The effluent was monitored by UV detection at 254 nm. Calibration plots were linear in the range 160 to 240 μg mL–1 and the LOD and LOQ were 14.26 and 41.21 μg mL–1, respectively. The high recovery and low relative standard deviation confirm the suitability of the method for routine QC determination of oxaprozin in tablets.
ProCite
RefWorks
Reference Manager
BibTeX
Zotero
EndNote
-
[1]. Merck Research Laboratories 2001 The Merck Index, An Encyclopedia of Chemical, Drugs, and Biologicals 11th edn Merck Research Laboratories Whitehouse Station, NJ, 6879, USA 1095.
-
[3]. K.V.S.R.K. Reddy D.S. Rao K. Vyas G.O. Reddy 2000 J. Pharm. Biomed. Anal. 22 651.
-
[4]. D.M. Pierce 1981 Xenobiotica 11 857.
-
[5]. F.W. Janssen S.K. Kirkman J.A. Knowles H.W. Ruelius 1978 Drug Metab. Dispos. 6 465.
-
[6]. L.S. McHugh S.K. Kirkman J.A. Knowles A. John 1980 J. Pharm. Sci. 69 794.
-
[7]. R. Matlis D.J. Greenblat 1984 J. Chromatogr. 445 310.
-
[8]. M. Kruowski H. Thobe 1989 Agents Actions 27 458.
-
[9]. J.B. Gao W. Hae N.N. Zhang W. Wang 2003 Chin. J. Pharm. 33 3 132.
-
[10]. J.D. Johnson G.E. Van Buskirk 1998 J. Valid. Technol. 2 88.
-
[11]. L.R. Snyder J.J. Kirkland J.L. Glajch 1988 Practical HPLC Method Development Wiley-Interscience New York 402.
-
[12]. International Conference on the Harmonization of Technical Requirements for the Registration of Pharmaceuticals for Human Use (ICH) Q2B (1996). Validation of Analytical Procedures, Methodology, pp. 1–8.
-
[13]. US Pharmacopoeial Convention, United States Pharmacopoeia, 28th edn, US Pharmacopoeial Convention, Rockville, MD, 2005, pp. 1196–1198.
-
[14]. FDA: Guidance for Industry, Analytical Procedures and Methods Validation, 2000.
Senior editors
Editor(s)-in-Chief: Sajewicz, Mieczyslaw, University of Silesia, Katowice, Poland
Editors(s)
- Danica Agbaba, University of Belgrade, Belgrade, Serbia (1953-2024)
- Łukasz Komsta, Medical University of Lublin, Lublin, Poland
- Ivana Stanimirova-Daszykowska, University of Silesia, Katowice, Poland
- Monika Waksmundzka-Hajnos, Medical University of Lublin, Lublin, Poland
Editorial Board
- Ravi Bhushan, The Indian Institute of Technology, Roorkee, India
- Jacek Bojarski, Jagiellonian University, Kraków, Poland
- Bezhan Chankvetadze, State University of Tbilisi, Tbilisi, Georgia
- Michał Daszykowski, University of Silesia, Katowice, Poland
- Tadeusz H. Dzido, Medical University of Lublin, Lublin, Poland
- Attila Felinger, University of Pécs, Pécs, Hungary
- Kazimierz Glowniak, Medical University of Lublin, Lublin, Poland
- Bronisław Glód, Siedlce University of Natural Sciences and Humanities, Siedlce, Poland
- Anna Gumieniczek, Medical University of Lublin, Lublin, Poland
- Urszula Hubicka, Jagiellonian University, Kraków, Poland
- Krzysztof Kaczmarski, Rzeszow University of Technology, Rzeszów, Poland
- Huba Kalász, Semmelweis University, Budapest, Hungary
- Katarina Karljiković Rajić, University of Belgrade, Belgrade, Serbia
- Imre Klebovich, Semmelweis University, Budapest, Hungary
- Angelika Koch, Private Pharmacy, Hamburg, Germany
- Piotr Kus, Univerity of Silesia, Katowice, Poland
- Debby Mangelings, Free University of Brussels, Brussels, Belgium
- Emil Mincsovics, Corvinus University of Budapest, Budapest, Hungary
- Ágnes M. Móricz, Centre for Agricultural Research, Budapest, Hungary
- Gertrud Morlock, Giessen University, Giessen, Germany
- Anna Petruczynik, Medical University of Lublin, Lublin, Poland
- Robert Skibiński, Medical University of Lublin, Lublin, Poland
- Bernd Spangenberg, Offenburg University of Applied Sciences, Germany
- Tomasz Tuzimski, Medical University of Lublin, Lublin, Poland
- Adam Voelkel, Poznań University of Technology, Poznań, Poland
- Beata Walczak, University of Silesia, Katowice, Poland
- Wiesław Wasiak, Adam Mickiewicz University, Poznań, Poland
- Igor G. Zenkevich, St. Petersburg State University, St. Petersburg, Russian Federation
SAJEWICZ, MIECZYSLAW
E-mail:mieczyslaw.sajewicz@us.edu.pl
Indexing and Abstracting Services:
- Science Citation Index
- Sci Search
- Research Alert
- Chemistry Citation Index and Current Content/Physical
- Chemical and Earth Sciences
- SCOPUS
- GoogleScholar
- Index Copernicus
- CABI
- CABELLS Journalytics
| 2023 | |
|---|---|
| Web of Science | |
| Journal Impact Factor | 1.7 |
| Rank by Impact Factor | Q3 (Chemistry, Analytical) |
| Journal Citation Indicator | 0.43 |
| Scopus | |
| CiteScore | 4.0 |
| CiteScore rank | Q2 (General Chemistry) |
| SNIP | 0.706 |
| Scimago | |
| SJR index | 0.344 |
| SJR Q rank | Q3 |
| Acta Chromatographica | |
|---|---|
| Publication Model | Online only Gold Open Access |
| Submission Fee | none |
| Article Processing Charge | 400 EUR/article Effective from 1st Feb 2025: 700 EUR/article |
| Regional discounts on country of the funding agency | World Bank Lower-middle-income economies: 50% World Bank Low-income economies: 100% |
| Further Discounts | Editorial Board / Advisory Board members: 50% Corresponding authors, affiliated to an EISZ member institution subscribing to the journal package of Akadémiai Kiadó: 100% |
| Subscription Information | Gold Open Access |
| Purchase per Title | |
| Acta Chromatographica | |
|---|---|
| Language | English |
| Size | A4 |
| Year of Foundation |
1988 |
| Volumes per Year |
1 |
| Issues per Year |
4 |
| Founder | Institute of Chemistry, University of Silesia |
| Founder's Address |
PL-40-007 Katowice, Poland, Bankowa 12 |
| Publisher | Akadémiai Kiadó |
| Publisher's Address |
H-1117 Budapest, Hungary 1516 Budapest, PO Box 245. |
| Responsible Publisher |
Chief Executive Officer, Akadémiai Kiadó |
| ISSN | 2083-5736 (Online) |
Monthly Content Usage
| Abstract Views | Full Text Views | PDF Downloads | |
|---|---|---|---|
| Aug 2024 | 0 | 14 | 8 |
| Sep 2024 | 0 | 34 | 2 |
| Oct 2024 | 0 | 103 | 2 |
| Nov 2024 | 0 | 84 | 2 |
| Dec 2024 | 0 | 67 | 4 |
| Jan 2025 | 0 | 17 | 2 |
| Feb 2025 | 0 | 0 | 0 |
Authors:
, , , , , , and
Authors:
, , , , , , and
Copyright Akadémiai Kiadó AKJournals is the trademark of Akadémiai Kiadó's journal publishing business branch.
Powered by PubFactory