Summary
A simple reversed-phase high-performance liquid chromatographic (RP-HPLC) method has been developed and validated for simultaneous analysis of three triterpene acids (corosolic, oleanolic, and ursolic acids) in extracts from inflorescences, leaves, and fruits of Prunus serotina Ehrh. (American black cherry). Separation of the acids was accomplished on a C18 column (5 μm, 250 mm × 4.6 mm i.d.) and recorded at 210 nm. The greatest resolution was achieved with 90:10 (υ/υ) methanol-1% aqueous orthophosphoric acid as mobile phase at a flow rate of 0.6 mL min−1. The correlation coefficients for all the calibration plots (r > 0.998) showed linearity good over the range tested. The relative standard deviation of the method was less than 3.3% for intra and inter-day assays, and average recovery was between 95.9 and 100.9%. Sensitivity was high; detection limits were between 0.034 and 0.067 μg mL−1. Total amounts of triterpene acids were 0.451–0.928, 0.031, and 0.911–1.455% in the inflorescences, fruits, and leaves of P. serotina, depending on the time of harvesting.
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[1]. A. Rehder 1947 Manual of Cultivated Trees and Shrubs, Hardy in North America Exclusive of Subtropical and Warmer Temperate Regions Macmillan New York 477.
-
[2]. A. Ordaz-Galindo P. Wesche-Ebeling R.E. Wrolstad L. Rodriguez-Saona A. Argaiz-Jamet 1999 Food Chem. 65 201.
-
[3]. J.E.F. Reynolds 1989 Martindale, The Extra Pharmacopoeia XXIX The Pharmaceutical Press London 1629.
-
[4]. A. Osol G.E. Farrar K.B. Beyer J.H. Brown D.K. Detweiler R. Pratt H.W. Youngken H.C. Wood 1995 The Dispensatory of the United States of America J.B. Lippincott Philadelphia, Montreal 273–275.
-
[5]. H.W.A. Biesseles A.C. van der Kerk-van Hoof J.J. Kettenes-van den Bosch C.A. Salemnik 1974 Phytochemistry 13 203.
-
[6]. F.B. Power C.W. Moore 1910 J. Chem. Soc. 97 1099.
-
[7]. M. Olszewska 2007 Acta Chromatogr. 19 253.
-
[8]. A.M. Diaz M.J. Abad L. Fernandez C. Recuero L. Villaescusa A. Silvan P. Bermejo 2000 Biol. Pharm. Bull. 23 1307.
-
[9]. E. Nadinic S. Gorzalczany A. Rojo C. van Baren S. Debenedetti C. Acevedo 1999 Fitoterapia 70 166.
-
[10]. R.M.E. Richards D.G. Durham X. Liu 1994 Planta Med. 60 471.
-
[11]. G.M. Woldemichael M.P. Singh W.M. Maiese B.M. Timmermann 2003 Z. Naturforsch. 58c 70.
-
[12]. Y. Kashiwada T. Nagao A. Hashimoto Y. Ikeshiro H. Okabe L.M. Cosentino K.H. Lee 2000 J. Nat. Prod. 63 1619.
-
[13]. E.C. Torres-Santos D. Lopes R. Rodrigues Oliveira J.P.P. Carauta C.A. Bandeira Falcao M.A.C. Kaplan B. Rossi-Bergmann 2004 Phytomedicine 11 114.
-
[14]. J. Liu 1995 J. Ethnopharmacol. 49 57.
-
[15]. L.I. Somowa A. Nadar P. Rammanan F.O. Shode 2003 Phytomedicine 10 115.
-
[16]. H.G. Jeong 1995 Toxicol. Lett. 105 215.
-
[17]. C. Farina M. Pinza G. Pifferi 1998 Farmaco 53 22.
-
[18]. M.C. Aguirre C. Delporte N. Backhouse S. Erazo M.E. Letelier B.K. Cassels X. Silva S. Alegria R. Negrete 2006 Bioorg. Med. Chem. 14 5673.
-
[19]. C.-M. Ma S.-Q. Cai J.-R. Cui R.-Q. Wang P.-F. Tu M. Hattori M. Daneshtalab 2005 Eur. J. Med. Chem. 40 582.
-
[20]. L. Shi W. Zhang Y.Y. Zhou Y.N. Zhang J.Y. Li L.H. Hu J. Li 2008 Eur. J. Pharm. 584 21.
-
[21]. X. Wen J. Xia K. Cheng L. Zhang P. Zhang J. Liu L. Zhang P. Ni H. Sun 2007 Bioorg. Med. Chem. Lett. 17 5777.
-
[22]. K. Yamada M. Hosokawa S. Fujimoto H. Fujiwara Y. Fujita N. Harada C. Yamada M. Fukushima N. Ueda T. Kaneko F. Matsuyama Y. Yamada Y. Seino N. Inagaki 2008 Diab. Res. Clin. Pract. 80 48.
-
[23]. Y. Yamaguchi K. Yamada N. Yoshikawa K. Nakamura J. Haginaka M. Kunitomo 2006 Life Sci. 79 2474.
-
[24]. G. Janicsak M. Veres M. Kallai I. Mathe 2003 Chromatographia 58 295.
-
[25]. M.C. Perez-Camino A. Cert 1999 J. Agric. Food Chem. 47 1558.
-
[26]. G. Takeoka L. Dao R. Teranishi R. Wong S. Flessa L. Harden R. Edwards 2000 J. Agric. Food Chem. 48 3437.
-
[27]. J.H. Chen Z.H. Xia R.X. Tan 2003 J. Pharm. Biomed. Anal. 32 1175.
-
[28]. B. Claude P. Morin M. Lafosse P. Andre 2004 J. Chromatogr. A 1049 37.
-
[29]. J.P. Fan C.H. He 2006 J. Pharm. Biomed. Anal. 41 950.
-
[30]. F. Gbaguidi G. Accrombessi M. Moudachirou J. Quetin-Leclercq 2005 J. Pharm. Biomed. Anal. 39 990.
-
[31]. L. Novotny M.E. Abdel-Hamid H. Hamza I. Masterova D. Grancai 2003 J. Pharm. Biomed. Anal. 31 961.
-
[32]. C. Zhou K. Chen C. Sun Q. Chen W. Zhang X. Li 2007 Biomed. Chromatogr. 21 755.
-
[33]. M.C.H. Tavares J.H. Yariwake Vigelas F.M. Lancas 2001 Phytochem. Anal. 12 134.
-
[34]. P. Yang Y. Li X. Liu S. Jiang 2007 J. Pharm. Biomed. Anal. 43 1331.
-
[35]. H. Liu Y. Shi D. Wang G. Yang A. Yu H. Zhang 2003 J. Pharm. Biomed. Anal. 32 479.
-
[36]. D.H. Kim K.M. Han I.S. Chung D.K. Kim S.H. Kim B.M. Kwon T.S. Jeong M.H. Park E.M. Ahn N.I. Baek 2005 Arch. Pharm. Res. 28 550.
-
[37]. Y.L. Li G. Wang J.Y. Xue Y.Z. Cen 2007 Zhongguo Zhong Yao Za Zhi 32 605.
-
[38]. P. Liu H.Q. Duan Q. Pan Y.W. Zhang Z. Yao 2006 Zhongguo Zhong Yao Za Zhi 31 1875.
-
[39]. S. Taniguchi Y. Imayoshi E. Kobayashi Y. Takamatsu H. Ito T. Hatano H. Sagatami H. Tokuda H. Nishino D. Sugita S. Shimura T. Yoshida 2002 Phytochemistry 59 315.
-
[40]. P.T. Tuong B.S. Min W. Jin M. Na J. Lee R. Seong Y.M. Lee K. Song Y. Seong H.K. Lee K. Ba S.S. Kang 2006 Biol. Pharm. Bull. 29 830.
-
[41]. S.B. Mahato A.P. Kundu 1994 Phytochemistry 37 1517.
-
[42]. H. Kojima H. Ogura 1989 Phytochemistry 28 1703.
-
[43]. L.R. Snyder J.J. Kirkland J.L. Glajch 1988 Practical HPLC Method Development 2 Wiley New York 23–27.
Senior editors
Editor(s)-in-Chief: Kowalska, Teresa
Editor(s)-in-Chief: Sajewicz, Mieczyslaw
Editors(s)
- Danica Agbaba (University of Belgrade, Belgrade, Serbia)
- Łukasz Komsta (Medical University of Lublin, Lublin, Poland)
- Ivana Stanimirova-Daszykowska (University of Silesia, Katowice, Poland)
- Monika Waksmundzka-Hajnos (Medical University of Lublin, Lublin, Poland)
Editorial Board
- R. Bhushan (The Indian Institute of Technology, Roorkee, India)
- J. Bojarski (Jagiellonian University, Kraków, Poland)
- B. Chankvetadze (State University of Tbilisi, Tbilisi, Georgia)
- M. Daszykowski (University of Silesia, Katowice, Poland)
- T.H. Dzido (Medical University of Lublin, Lublin, Poland)
- A. Felinger (University of Pécs, Pécs, Hungary)
- K. Glowniak (Medical University of Lublin, Lublin, Poland)
- B. Glód (Siedlce University of Natural Sciences and Humanities, Siedlce, Poland)
- A. Gumieniczek (Medical University of Lublin, Lublin, Poland)
- U. Hubicka (Jagiellonian University, Kraków, Poland)
- K. Kaczmarski (Rzeszow University of Technology, Rzeszów, Poland)
- H. Kalász (Semmelweis University, Budapest, Hungary)
- K. Karljiković Rajić (University of Belgrade, Belgrade, Serbia)
- I. Klebovich (Semmelweis University, Budapest, Hungary)
- A. Koch (Private Pharmacy, Hamburg, Germany)
- P. Kus (Univerity of Silesia, Katowice, Poland)
- D. Mangelings (Free University of Brussels, Brussels, Belgium)
- E. Mincsovics (Corvinus University of Budapest, Budapest, Hungary)
- Á. M. Móricz (Centre for Agricultural Research, Budapest, Hungary)
- G. Morlock (Giessen University, Giessen, Germany)
- A. Petruczynik (Medical University of Lublin, Lublin, Poland)
- R. Skibiński (Medical University of Lublin, Lublin, Poland)
- B. Spangenberg (Offenburg University of Applied Sciences, Germany)
- T. Tuzimski (Medical University of Lublin, Lublin, Poland)
- Y. Vander Heyden (Free University of Brussels, Brussels, Belgium)
- A. Voelkel (Poznań University of Technology, Poznań, Poland)
- B. Walczak (University of Silesia, Katowice, Poland)
- W. Wasiak (Adam Mickiewicz University, Poznań, Poland)
- I.G. Zenkevich (St. Petersburg State University, St. Petersburg, Russian Federation)
KOWALSKA, TERESA
E-mail: kowalska@us.edu.pl
SAJEWICZ, MIECZYSLAW
E-mail:msajewic@us.edu.pl
Indexing and Abstracting Services:
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| 2021 | |
|---|---|
| Web of Science | |
| Total Cites WoS |
652 |
| Journal Impact Factor | 2,011 |
| Rank by Impact Factor | Chemistry, Analytical 66/87 |
| Impact Factor without Journal Self Cites |
1,789 |
| 5 Year Impact Factor |
1,350 |
| Journal Citation Indicator | 0,40 |
| Rank by Journal Citation Indicator | Chemistry, Analytical 72/99 |
| Scimago | |
| Scimago H-index |
29 |
| Scimago Journal Rank |
0,27 |
| Scimago Quartile Score | Chemistry (miscellaneous) (Q3) |
| Scopus | |
| Scopus Cite Score |
2,8 |
| Scopus CIte Score Rank |
General Chemistry 210/409 (Q3) |
| Scopus SNIP |
0,586 |
|
2020
|
|
|
Total Cites
|
650
|
|
WoS
|
|
|
Journal
Impact Factor |
1,639
|
|
Rank by
|
Chemistry, Analytical 71/83 (Q4)
|
|
Impact Factor
|
|
|
Impact Factor
|
1,412
|
|
without
|
|
|
Journal Self Cites
|
|
|
5 Year
|
1,301
|
|
Impact Factor
|
|
|
Journal
|
0,34
|
|
Citation Indicator
|
|
|
Rank by Journal
|
Chemistry, Analytical 75/93 (Q4)
|
|
Citation Indicator
|
|
|
Citable
|
45
|
|
Items
|
|
|
Total
|
43
|
|
Articles
|
|
|
Total
|
2
|
|
Reviews
|
|
|
Scimago
|
28
|
|
H-index
|
|
|
Scimago
|
0,316
|
|
Journal Rank
|
|
|
Scimago
|
Chemistry (miscellaneous) Q3
|
|
Quartile Score
|
|
|
Scopus
|
393/181=2,2
|
|
Scite Score
|
|
|
Scopus
|
General Chemistry 215/398 (Q3)
|
|
Scite Score Rank
|
|
|
Scopus
|
0,560
|
|
SNIP
|
|
|
Days from
|
58
|
|
submission
|
|
|
to acceptance
|
|
|
Days from
|
68
|
|
acceptance
|
|
|
to publication
|
|
|
Acceptance
|
51%
|
| Rate |
| 2019 | |
|---|---|
| Total Cites WoS |
495 |
| Impact Factor | 1,418 |
| Impact Factor without Journal Self Cites |
1,374 |
| 5 Year Impact Factor |
0,936 |
| Immediacy Index |
0,460 |
| Citable Items |
50 |
| Total Articles |
50 |
| Total Reviews |
0 |
| Cited Half-Life |
6,2 |
| Citing Half-Life |
8,3 |
| Eigenfactor Score |
0,00048 |
| Article Influence Score |
0,164 |
| % Articles in Citable Items |
100,00 |
| Normalized Eigenfactor |
0,05895 |
| Average IF Percentile |
20,349 |
| Scimago H-index |
26 |
| Scimago Journal Rank |
0,255 |
| Scopus Scite Score |
226/167=1,4 |
| Scopus Scite Score Rank |
Chemistry (miscellaneous) 240/398 (Q3) |
| Scopus SNIP |
0,494 |
| Acceptance Rate |
41% |
| Acta Chromatographica | |
|---|---|
| Publication Model | Online only Gold Open Access |
| Submission Fee | none |
| Article Processing Charge | 400 EUR/article |
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| Subscription Information | Gold Open Access |
| Purchase per Title | |
| Acta Chromatographica | |
|---|---|
| Language | English |
| Size | A4 |
| Year of Foundation |
1988 |
| Volumes per Year |
1 |
| Issues per Year |
4 |
| Founder | Institute of Chemistry, University of Silesia |
| Founder's Address |
PL-40-007 Katowice, Poland, Bankowa 12 |
| Publisher | Akadémiai Kiadó |
| Publisher's Address |
H-1117 Budapest, Hungary 1516 Budapest, PO Box 245. |
| Responsible Publisher |
Chief Executive Officer, Akadémiai Kiadó |
| ISSN | 2083-5736 (Online) |
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