View More View Less
  • 1 Department of Pharmacognosy, Faculty of Pharmacy, Medical University of Łódź, 1 Muszyński St, 90-151, Łódź, Poland
Full access

Summary

A simple reversed-phase high-performance liquid chromatographic (RP-HPLC) method has been developed and validated for simultaneous analysis of three triterpene acids (corosolic, oleanolic, and ursolic acids) in extracts from inflorescences, leaves, and fruits of Prunus serotina Ehrh. (American black cherry). Separation of the acids was accomplished on a C18 column (5 μm, 250 mm × 4.6 mm i.d.) and recorded at 210 nm. The greatest resolution was achieved with 90:10 (υ/υ) methanol-1% aqueous orthophosphoric acid as mobile phase at a flow rate of 0.6 mL min−1. The correlation coefficients for all the calibration plots (r > 0.998) showed linearity good over the range tested. The relative standard deviation of the method was less than 3.3% for intra and inter-day assays, and average recovery was between 95.9 and 100.9%. Sensitivity was high; detection limits were between 0.034 and 0.067 μg mL−1. Total amounts of triterpene acids were 0.451–0.928, 0.031, and 0.911–1.455% in the inflorescences, fruits, and leaves of P. serotina, depending on the time of harvesting.

  • [1]. A. Rehder 1947 Manual of Cultivated Trees and Shrubs, Hardy in North America Exclusive of Subtropical and Warmer Temperate Regions Macmillan New York 477.

    • Search Google Scholar
    • Export Citation
  • [2]. A. Ordaz-Galindo P. Wesche-Ebeling R.E. Wrolstad L. Rodriguez-Saona A. Argaiz-Jamet 1999 Food Chem. 65 201.

  • [3]. J.E.F. Reynolds 1989 Martindale, The Extra Pharmacopoeia XXIX The Pharmaceutical Press London 1629.

  • [4]. A. Osol G.E. Farrar K.B. Beyer J.H. Brown D.K. Detweiler R. Pratt H.W. Youngken H.C. Wood 1995 The Dispensatory of the United States of America J.B. Lippincott Philadelphia, Montreal 273275.

    • Search Google Scholar
    • Export Citation
  • [5]. H.W.A. Biesseles A.C. van der Kerk-van Hoof J.J. Kettenes-van den Bosch C.A. Salemnik 1974 Phytochemistry 13 203.

  • [6]. F.B. Power C.W. Moore 1910 J. Chem. Soc. 97 1099.

  • [7]. M. Olszewska 2007 Acta Chromatogr. 19 253.

  • [8]. A.M. Diaz M.J. Abad L. Fernandez C. Recuero L. Villaescusa A. Silvan P. Bermejo 2000 Biol. Pharm. Bull. 23 1307.

  • [9]. E. Nadinic S. Gorzalczany A. Rojo C. van Baren S. Debenedetti C. Acevedo 1999 Fitoterapia 70 166.

  • [10]. R.M.E. Richards D.G. Durham X. Liu 1994 Planta Med. 60 471.

  • [11]. G.M. Woldemichael M.P. Singh W.M. Maiese B.M. Timmermann 2003 Z. Naturforsch. 58c 70.

  • [12]. Y. Kashiwada T. Nagao A. Hashimoto Y. Ikeshiro H. Okabe L.M. Cosentino K.H. Lee 2000 J. Nat. Prod. 63 1619.

  • [13]. E.C. Torres-Santos D. Lopes R. Rodrigues Oliveira J.P.P. Carauta C.A. Bandeira Falcao M.A.C. Kaplan B. Rossi-Bergmann 2004 Phytomedicine 11 114.

    • Search Google Scholar
    • Export Citation
  • [14]. J. Liu 1995 J. Ethnopharmacol. 49 57.

  • [15]. L.I. Somowa A. Nadar P. Rammanan F.O. Shode 2003 Phytomedicine 10 115.

  • [16]. H.G. Jeong 1995 Toxicol. Lett. 105 215.

  • [17]. C. Farina M. Pinza G. Pifferi 1998 Farmaco 53 22.

  • [18]. M.C. Aguirre C. Delporte N. Backhouse S. Erazo M.E. Letelier B.K. Cassels X. Silva S. Alegria R. Negrete 2006 Bioorg. Med. Chem. 14 5673.

    • Search Google Scholar
    • Export Citation
  • [19]. C.-M. Ma S.-Q. Cai J.-R. Cui R.-Q. Wang P.-F. Tu M. Hattori M. Daneshtalab 2005 Eur. J. Med. Chem. 40 582.

  • [20]. L. Shi W. Zhang Y.Y. Zhou Y.N. Zhang J.Y. Li L.H. Hu J. Li 2008 Eur. J. Pharm. 584 21.

  • [21]. X. Wen J. Xia K. Cheng L. Zhang P. Zhang J. Liu L. Zhang P. Ni H. Sun 2007 Bioorg. Med. Chem. Lett. 17 5777.

  • [22]. K. Yamada M. Hosokawa S. Fujimoto H. Fujiwara Y. Fujita N. Harada C. Yamada M. Fukushima N. Ueda T. Kaneko F. Matsuyama Y. Yamada Y. Seino N. Inagaki 2008 Diab. Res. Clin. Pract. 80 48.

    • Search Google Scholar
    • Export Citation
  • [23]. Y. Yamaguchi K. Yamada N. Yoshikawa K. Nakamura J. Haginaka M. Kunitomo 2006 Life Sci. 79 2474.

  • [24]. G. Janicsak M. Veres M. Kallai I. Mathe 2003 Chromatographia 58 295.

  • [25]. M.C. Perez-Camino A. Cert 1999 J. Agric. Food Chem. 47 1558.

  • [26]. G. Takeoka L. Dao R. Teranishi R. Wong S. Flessa L. Harden R. Edwards 2000 J. Agric. Food Chem. 48 3437.

  • [27]. J.H. Chen Z.H. Xia R.X. Tan 2003 J. Pharm. Biomed. Anal. 32 1175.

  • [28]. B. Claude P. Morin M. Lafosse P. Andre 2004 J. Chromatogr. A 1049 37.

  • [29]. J.P. Fan C.H. He 2006 J. Pharm. Biomed. Anal. 41 950.

  • [30]. F. Gbaguidi G. Accrombessi M. Moudachirou J. Quetin-Leclercq 2005 J. Pharm. Biomed. Anal. 39 990.

  • [31]. L. Novotny M.E. Abdel-Hamid H. Hamza I. Masterova D. Grancai 2003 J. Pharm. Biomed. Anal. 31 961.

  • [32]. C. Zhou K. Chen C. Sun Q. Chen W. Zhang X. Li 2007 Biomed. Chromatogr. 21 755.

  • [33]. M.C.H. Tavares J.H. Yariwake Vigelas F.M. Lancas 2001 Phytochem. Anal. 12 134.

  • [34]. P. Yang Y. Li X. Liu S. Jiang 2007 J. Pharm. Biomed. Anal. 43 1331.

  • [35]. H. Liu Y. Shi D. Wang G. Yang A. Yu H. Zhang 2003 J. Pharm. Biomed. Anal. 32 479.

  • [36]. D.H. Kim K.M. Han I.S. Chung D.K. Kim S.H. Kim B.M. Kwon T.S. Jeong M.H. Park E.M. Ahn N.I. Baek 2005 Arch. Pharm. Res. 28 550.

  • [37]. Y.L. Li G. Wang J.Y. Xue Y.Z. Cen 2007 Zhongguo Zhong Yao Za Zhi 32 605.

  • [38]. P. Liu H.Q. Duan Q. Pan Y.W. Zhang Z. Yao 2006 Zhongguo Zhong Yao Za Zhi 31 1875.

  • [39]. S. Taniguchi Y. Imayoshi E. Kobayashi Y. Takamatsu H. Ito T. Hatano H. Sagatami H. Tokuda H. Nishino D. Sugita S. Shimura T. Yoshida 2002 Phytochemistry 59 315.

    • Search Google Scholar
    • Export Citation
  • [40]. P.T. Tuong B.S. Min W. Jin M. Na J. Lee R. Seong Y.M. Lee K. Song Y. Seong H.K. Lee K. Ba S.S. Kang 2006 Biol. Pharm. Bull. 29 830.

    • Search Google Scholar
    • Export Citation
  • [41]. S.B. Mahato A.P. Kundu 1994 Phytochemistry 37 1517.

  • [42]. H. Kojima H. Ogura 1989 Phytochemistry 28 1703.

  • [43]. L.R. Snyder J.J. Kirkland J.L. Glajch 1988 Practical HPLC Method Development 2 Wiley New York 2327.

The author instruction is available in PDF.
Please, download the file from HERE.
 
The Open Access statement together with the description of the Copyright and License Policy are available in PDF.
Please, download the file from HERE.
 

 

Senior editors

Editor(s)-in-Chief: Kowalska, Teresa

Editor(s)-in-Chief: Sajewicz, Mieczyslaw

Editors(s)

  • Danica Agbaba (University of Belgrade, Belgrade, Serbia)
  • Ivana Stanimirova-Daszykowska (University of Silesia, Katowice, Poland)
  • Monika Waksmundzka-Hajnos (Medical University of Lublin, Lublin, Poland)

Editorial Board

  • R. Bhushan (The Indian Institute of Technology, Roorkee, India)
  • J. Bojarski (Jagiellonian University, Kraków, Poland)
  • B. Chankvetadze (State University of Tbilisi, Tbilisi, Georgia)
  • M. Daszykowski (University of Silesia, Katowice, Poland)
  • T.H. Dzido (Medical University of Lublin, Lublin, Poland)
  • A. Felinger (University of Pécs, Pécs, Hungary)
  • K. Glowniak (Medical University of Lublin, Lublin, Poland)
  • B. Glód (Siedlce University of Natural Sciences and Humanities, Siedlce, Poland)
  • A. Gumieniczek (Medical University of Lublin, Lublin, Poland)
  • U. Hubicka (Jagiellonian University, Kraków, Poland)
  • K. Kaczmarski (Rzeszow University of Technology, Rzeszów, Poland)
  • H. Kalász (Semmelweis University, Budapest, Hungary)
  • I. Klebovich (Semmelweis University, Budapest, Hungary)
  • A. Koch (Private Pharmacy, Hamburg, Germany)
  • Ł. Komsta (Medical University of Lublin, Lublin, Poland)
  • P. Kus (Univerity of Silesia, Katowice, Poland)
  • D. Mangelings (Free University of Brussels, Brussels, Belgium)
  • E. Mincsovics (Corvinus University of Budapest, Budapest, Hungary)
  • G. Morlock (Giessen University, Giessen, Germany)
  • A. Petruczynik (Medical University of Lublin, Lublin, Poland)
  • J. Sherma (Lafayette College, Easton, PA, USA)
  • R. Skibiński (Medical University of Lublin, Lublin, Poland)
  • B. Spangenberg (Offenburg University of Applied Sciences, Germany)
  • T. Tuzimski (Medical University of Lublin, Lublin, Poland)
  • Y. Vander Heyden (Free University of Brussels, Brussels, Belgium)
  • A. Voelkel (Poznań University of Technology, Poznań, Poland)
  • B. Walczak (University of Silesia, Katowice, Poland)
  • W. Wasiak (Adam Mickiewicz University, Poznań, Poland)

 

KOWALSKA, TERESA
E-mail: kowalska@us.edu.pl

SAJEWICZ, MIECZYSLAW
E-mail:msajewic@us.edu.pl

Indexing and Abstracting Services:

  • Science Citation Index
  • Sci Search
  • Research Alert
  • Chemistry Citation Index and Current Content/Physical
  • Chemical and Earth Sciences
  • SCOPUS
  • GoogleScholar
  • Index Copernicus
  • CABI
2020
 
Total Cites
650
WoS
Journal
Impact Factor
1,639
Rank by
Chemistry, Analytical 71/83 (Q4)
Impact Factor
 
Impact Factor
1,412
without
Journal Self Cites
5 Year
1,301
Impact Factor
Journal
0,34
Citation Indicator
 
Rank by Journal
Chemistry, Analytical 75/93 (Q4)
Citation Indicator
 
Citable
45
Items
Total
43
Articles
Total
2
Reviews
Scimago
28
H-index
Scimago
0,316
Journal Rank
Scimago
Chemistry (miscellaneous) Q3
Quartile Score
 
Scopus
393/181=2,2
Scite Score
 
Scopus
General Chemistry 215/398 (Q3)
Scite Score Rank
 
Scopus
0,560
SNIP
 
Days from
58
submission
 
to acceptance
 
Days from
68
acceptance
 
to publication
 
Acceptance
51%
Rate

2019  
Total Cites
WoS
495
Impact Factor 1,418
Impact Factor
without
Journal Self Cites
1,374
5 Year
Impact Factor
0,936
Immediacy
Index
0,460
Citable
Items
50
Total
Articles
50
Total
Reviews
0
Cited
Half-Life
6,2
Citing
Half-Life
8,3
Eigenfactor
Score
0,00048
Article Influence
Score
0,164
% Articles
in
Citable Items
100,00
Normalized
Eigenfactor
0,05895
Average
IF
Percentile
20,349
Scimago
H-index
26
Scimago
Journal Rank
0,255
Scopus
Scite Score
226/167=1,4
Scopus
Scite Score Rank
Chemistry (miscellaneous) 240/398 (Q3)
Scopus
SNIP
0,494
Acceptance
Rate
41%

 

Acta Chromatographica
Publication Model Online only
Gold Open Access
Submission Fee none
Article Processing Charge 400 EUR/article
Regional discounts on country of the funding agency World Bank Lower-middle-income economies: 50%
World Bank Low-income economies: 100%
Further Discounts Editorial Board / Advisory Board members: 50%
Corresponding authors, affiliated to an EISZ member institution subscribing to the journal package of Akadémiai Kiadó: 100%
Subscription Information Gold Open Access
Purchase per Title  

Acta Chromatographica
Language English
Size A4
Year of
Foundation
1992
Volumes
per Year
1
Issues
per Year
4
Founder Institute of Chemistry, University of Silesia
Founder's
Address
PL-40-007 Katowice, Poland, Bankowa 12
Publisher Akadémiai Kiadó
Publisher's
Address
H-1117 Budapest, Hungary 1516 Budapest, PO Box 245.
Responsible
Publisher
Chief Executive Officer, Akadémiai Kiadó
ISSN 2083-5736 (Online)

Monthly Content Usage

Abstract Views Full Text Views PDF Downloads
Aug 2021 0 6 5
Sep 2021 0 3 0
Oct 2021 0 5 11
Nov 2021 0 6 5
Dec 2021 0 1 1
Jan 2022 0 4 4
Feb 2022 0 0 0