View More View Less
  • 1 Product Development Department, ICN Polfa Rzeszów S.A., 35-959, Rzeszów, Poland
  • | 2 Department of Chemical and Process Engineering, Rzeszów University of Technology, 35-959, Rzeszów, Poland
Full access

Summary

The new analytical method of very high pressure liquid chromatography (VHPLC) has been designed for the estimation of related substances in bisoprolol fumarate. Several columns filled with sub-2-μm totally porous and shell adsorbent have been tested and compared during the method development. The columns' resolution was investigated. The shell adsorbent appears to have smaller resolution than the totally porous adsorbent. The tips and recommendations for the HPLC-VHPLC method transfer are presented. Significant reduction in analysis run time and solvent consumption has been obtained.

  • [1]. J. Kirkland 1969 Anal. Chem. 41 218.

  • [2]. A. Cavazzini F. Gritti K. Kaczmarski N. Marchetti G. Guiochon 2007 Anal. Chem. 79 5972.

  • [3]. J.J. DeStefano T.J. Langlois J.J. Kirkland 2008 J. Chromatogr. Sci. 46 254.

  • [4]. F. Gritti G. Guiochon 2010 J. Chromatogr. A 1217 7677.

  • [5]. K. Kaczmarski G. Guiochon 2007 Anal. Chem. 79 4648.

  • [6]. J.W. Eschelbach J.W. Jorgenson 2006 Anal. Chem. 78 1697.

  • [7]. J. Mensch M. Noppe J. Adriaensen A. Melis C. Mackie P. Augustijns M.E. Brewster 2007 J. Chromatogr. B 847 182.

  • [8]. K. Horváth F. Gritti J.N. Fairchild G. Guiochon 2010 J. Chromatogr. A 1217 6373.

  • [9]. N. Marchetti A. Cavazzini F. Gritti G. Guiochon 2007 J. Chromatogr. A 1163 203.

  • [10]. F. Gritti G. Guiochon 2010 J. Chromatogr. A 1217 1604.

  • [11]. K. Kaczmarski J. Kostka W. Zapała G. Guiochon 2009 J. Chromatogr. A 1216 6560.

  • [12]. K. Kaczmarski F. Gritti J. Kostka G. Guiochon 2009 J. Chromatogr. A 1216 6575.

  • [13]. J. Kostka F. Gritti G. Guiochon K. Kaczmarski 2010 J. Chromatogr. A 1217 4704.

  • [14]. G. Guiochon A. Felinger A.M. Katti D. Shirazi 2006 Fundamentals of Preparative and Nonlinear Chromatography 2nd edn Elsevier Amsterdam.

    • Search Google Scholar
    • Export Citation
  • [15]. K. Kaczmarski 2011 J. Chromatogr. A 1218 951.

  • [16]. S. Williams 2004 J. Chromatogr. A 1052 1.

  • [17]. M. Swartz , HPLC to UPLC method migration, An overview of key considerations and available tools, 2007 Waters Corporation, http://wwwwaterscom/webassets/cms/library/docs/720002064enpdf.

    • Search Google Scholar
    • Export Citation
  • [18]. E.J. Wilson C.J. Geankoplis 1966 Ind. Eng. Chem. Fund. 5 9.

  • [19]. C.R. Wilke 1955 Chang P AIChE J 1 264.

  • [20]. C.Y. Wen L.T. Fan 1975 Models for Flow Systems and Chemical Reactors Marcel Dekker Inc New York 137.

  • [21]. R.B. Bird W.E. Stewart E.N. Lightfoot 2002 Transport Phenomena John Wiley & Sons New York.

The author instruction is available in PDF.
Please, download the file from HERE.
 
The Open Access statement together with the description of the Copyright and License Policy are available in PDF.
Please, download the file from HERE.
 

 

Senior editors

Editor(s)-in-Chief: Kowalska, Teresa

Editor(s)-in-Chief: Sajewicz, Mieczyslaw

Editors(s)

  • Danica Agbaba (University of Belgrade, Belgrade, Serbia)
  • Ivana Stanimirova-Daszykowska (University of Silesia, Katowice, Poland)
  • Monika Waksmundzka-Hajnos (Medical University of Lublin, Lublin, Poland)

Editorial Board

  • R. Bhushan (The Indian Institute of Technology, Roorkee, India)
  • J. Bojarski (Jagiellonian University, Kraków, Poland)
  • B. Chankvetadze (State University of Tbilisi, Tbilisi, Georgia)
  • M. Daszykowski (University of Silesia, Katowice, Poland)
  • T.H. Dzido (Medical University of Lublin, Lublin, Poland)
  • A. Felinger (University of Pécs, Pécs, Hungary)
  • K. Glowniak (Medical University of Lublin, Lublin, Poland)
  • B. Glód (Siedlce University of Natural Sciences and Humanities, Siedlce, Poland)
  • U. Hubicka (Jagiellonian University, Kraków, Poland)
  • K. Kaczmarski (Rzeszow University of Technology, Rzeszów, Poland)
  • H. Kalász (Semmelweis University, Budapest, Hungary)
  • I. Klebovich (Semmelweis University, Budapest, Hungary)
  • A. Koch (Private Pharmacy, Hamburg, Germany)
  • Ł. Komsta (Medical University of Lublin, Lublin, Poland)
  • P. Kus (Univerity of Silesia, Katowice, Poland)
  • D. Mangelings (Free University of Brussels, Brussels, Belgium)
  • E. Mincsovics (Corvinus University of Budapest, Budapest, Hungary)
  • G. Morlock (Giessen University, Giessen, Germany)
  • A. Petruczynik (Medical University of Lublin, Lublin, Poland)
  • J. Sherma (Lafayette College, Easton, PA, USA)
  • R. Skibiński (Medical University of Lublin, Lublin, Poland)
  • B. Spangenberg (Offenburg University of Applied Sciences, Germany)
  • T. Tuzimski (Medical University of Lublin, Lublin, Poland)
  • Y. Vander Heyden (Free University of Brussels, Brussels, Belgium)
  • A. Voelkel (Poznań University of Technology, Poznań, Poland)
  • B. Walczak (University of Silesia, Katowice, Poland)
  • W. Wasiak (Adam Mickiewicz University, Poznań, Poland)

 

KOWALSKA, TERESA
E-mail: kowalska@us.edu.pl

SAJEWICZ, MIECZYSLAW
E-mail:msajewic@us.edu.pl

Indexing and Abstracting Services:

  • Science Citation Index
  • Sci Search
  • Research Alert
  • Chemistry Citation Index and Current Content/Physical
  • Chemical and Earth Sciences
  • SCOPUS
  • GoogleScholar
  • Index Copernicus
  • CABI
2020
 
Total Cites
650
WoS
Journal
Impact Factor
1,639
Rank by
Chemistry, Analytical 71/83 (Q4)
Impact Factor
 
Impact Factor
1,412
without
Journal Self Cites
5 Year
1,301
Impact Factor
Journal
0,34
Citation Indicator
 
Rank by Journal
Chemistry, Analytical 75/93 (Q4)
Citation Indicator
 
Citable
45
Items
Total
43
Articles
Total
2
Reviews
Scimago
28
H-index
Scimago
0,316
Journal Rank
Scimago
Chemistry (miscellaneous) Q3
Quartile Score
 
Scopus
393/181=2,2
Scite Score
 
Scopus
General Chemistry 215/398 (Q3)
Scite Score Rank
 
Scopus
0,560
SNIP
 
Days from
58
submission
 
to acceptance
 
Days from
68
acceptance
 
to publication
 
Acceptance
51%
Rate

2019  
Total Cites
WoS
495
Impact Factor 1,418
Impact Factor
without
Journal Self Cites
1,374
5 Year
Impact Factor
0,936
Immediacy
Index
0,460
Citable
Items
50
Total
Articles
50
Total
Reviews
0
Cited
Half-Life
6,2
Citing
Half-Life
8,3
Eigenfactor
Score
0,00048
Article Influence
Score
0,164
% Articles
in
Citable Items
100,00
Normalized
Eigenfactor
0,05895
Average
IF
Percentile
20,349
Scimago
H-index
26
Scimago
Journal Rank
0,255
Scopus
Scite Score
226/167=1,4
Scopus
Scite Score Rank
Chemistry (miscellaneous) 240/398 (Q3)
Scopus
SNIP
0,494
Acceptance
Rate
41%

 

Acta Chromatographica
Publication Model Online only
Gold Open Access
Submission Fee none
Article Processing Charge 400 EUR/article
Regional discounts on country of the funding agency World Bank Lower-middle-income economies: 50%
World Bank Low-income economies: 100%
Further Discounts Editorial Board / Advisory Board members: 50%
Corresponding authors, affiliated to an EISZ member institution subscribing to the journal package of Akadémiai Kiadó: 100%
Subscription Information Gold Open Access
Purchase per Title  

Acta Chromatographica
Language English
Size A4
Year of
Foundation
1992
Publication
Programme
2021 Volume 33
Volumes
per Year
1
Issues
per Year
4
Founder Institute of Chemistry, University of Silesia
Founder's
Address
PL-40-007 Katowice, Poland, Bankowa 12
Publisher Akadémiai Kiadó
Publisher's
Address
H-1117 Budapest, Hungary 1516 Budapest, PO Box 245.
Responsible
Publisher
Chief Executive Officer, Akadémiai Kiadó
ISSN 2083-5736 (Online)

Monthly Content Usage

Abstract Views Full Text Views PDF Downloads
Jun 2021 18 0 0
Jul 2021 10 3 5
Aug 2021 0 3 15
Sep 2021 0 4 18
Oct 2021 0 3 29
Nov 2021 0 12 24
Dec 2021 0 0 0