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  • 1 Department of Environmental Studies, School of Environment and Natural Resources, Doon University, Dehradun, 248001, India
  • | 2 Department of Chemistry, K.L.D.A.V. (P.G.) College, Roorkee, 247667, India
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Summary

Enantiomeric resolution of two commonly used β-blockers, namely, (±)-propranolol and (±)-atenolol, has been achieved on silica gel layers which were bulkimpregnated with β-cyclodextrin. Solvent systems DMF-ethyl acetate-butanol (3:2:5, υ/υ) and butanol-acetic acid-ethyl acetate-ammonia (5:2:2:0.5, υ/υ) successfully resolved the enantiomers of (±)-propranolol and (±)-atenolol, respectively. The spots were located with iodine vapor. The effects of concentration of the chiral selector and mobile phase variation were also studied.

  • [1]. U. Borchard 1998 J. Clin. Cardiol. 1 59.

  • [2]. R. Mehvar D.R. Brocks 2001 J. Pharm. Pharmaceut. Sci. 4 185200.

  • [3]. A. Burger 1970 Medicinal Chemistry — Part II 3rd edn Wiley Interscience New York 1246.

  • [4]. M.H. Hyun 2006 J. Sep. Sci. 29 750761.

  • [5]. A. Ghanem H. Hoenen H.Y. Aboul-Enein 2006 Talanta 68 602609.

  • [6]. X. Zhang J. Ouyang W.R.G. Baryens S. Zhae Y. Yang G. Huang 2003 J. Pharm. Biomed. Anal. 31 10471057.

  • [7]. C. Vandenbosch D.L. Massart W. Lindner 1992 J. Pharm. Biomed. Anal. 10 895908.

  • [8]. B. Mistry J.L. Leslie N.D. Eddington 2001 J. Chromatogr. B 758 153161.

  • [9]. M.I.R.M. Santoro H.S. Cho E.R.M. Kedor-Hackmann 2001 Drug Dev. Ind. Pharm. 27 693697.

  • [10]. A.M. Dyas M.L. Robinson A.F. Fell 1991 J. Chromatogr. 586 351355.

  • [11]. P.V. Petersen J. Ekelund L. Olsen S.V. Ovsen 1999 J. Chromatogr. A 757 6571.

  • [12]. A. Ceccato Ph. Hubert J. Crommen 1997 J. Chromatogr. A 760 193203.

  • [13]. Y. Machida H. Nishi K. Nakamura H. Nakai T. Sato 1997 J. Chromatogr. A 757 7379.

  • [14]. K. Krause M. Girod B. Chankvetadze G. Blaschke 1999 J. Chromatogr. A 837 5163.

  • [15]. D. Agbaba B. Ivkovic 2007 T. Kowalska J. Sherma Thin Layer Chromatography in Chiral Separations and Analysis Taylor and Francis New York 283304.

    • Search Google Scholar
    • Export Citation
  • [16]. R. Bhushan C. Agrawal 2008 J. Planar Chromatogr. 21 129134.

  • [17]. R. Bhushan D. Gupta 2006 J. Planar Chromatogr. 19 241246.

  • [18]. R. Bhushan M. Arora 2003 Biomed. Chromatogr. 17 226230.

  • [19]. R. Bhushan G.T. Thiongo 1998 J. Chromatogr. B 708 330334.

  • [20]. R. Bhushan S. Tanwar 2008 Biomed. Chromatogr. 22 10281034.

  • [21]. M.B. Haung 1997 J. Liq. Chromatogr. Relat. Technol. 20 15071514.

  • [22]. R. Bhushan C. Agrawal 2010 J. Planar Chromatogr. 23 713.

  • [23]. M.V. Rekharsky Y. Inoue 1998 Chem. Rev. 98 18751917.

  • [24]. D.M. Radulovic K.D. Karljikovic-Rajic B.M. Lucic Z.B. Vujic 2001 J. Pharm. Biomed. Anal. 24 5–6 871876.

  • [25]. A.F. Danil de Namor R. Trabaulssi D.F.V. Lewis 1990 J. Am. Chem. Soc. 112 84428447.

  • [26]. B. Siegel R. Breslow 1975 J. Am. Chem. Soc. 97 68696870.

  • [27]. Y. Sueishi M. Kasahara M. Inoue K.J. Matsueda 2003 Inclusion Phenom. Macrocyclic Chem. 46 7175.

  • [28]. K.A. Cannors 1997 Chem. Rev. 97 1335357.

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Senior editors

Editor(s)-in-Chief: Kowalska, Teresa

Editor(s)-in-Chief: Sajewicz, Mieczyslaw

Editors(s) Danica Agbaba (University of Belgrade, Belgrade, Serbia);
Ivana Stanimirova-Daszykowska (University of Silesia, Katowice, Poland),
Monika Waksmundzka-Hajnos (Medical University of Lublin, Lublin, Poland)

Editorial Board

R. Bhushan (The Indian Institute of Technology, Roorkee, India)
J. Bojarski (Jagiellonian University, Kraków, Poland)
B. Chankvetadze (State University of Tbilisi, Tbilisi, Georgia)
M. Daszykowski (University of Silesia, Katowice, Poland)
T.H. Dzido (Medical University of Lublin, Lublin, Poland)
A. Felinger (University of Pécs, Pécs, Hungary)
K. Glowniak (Medical University of Lublin, Lublin, Poland)
B. Glód (Siedlce University of Natural Sciences and Humanities, Siedlce, Poland)
K. Kaczmarski (Rzeszow University of Technology, Rzeszów, Poland)
H. Kalász (Semmelweis University, Budapest, Hungary)
I. Klebovich (Semmelweis University, Budapest, Hungary)
A. Koch (Private Pharmacy, Hamburg, Germany)
Ł. Komsta (Medical University of Lublin, Lublin, Poland)
P. Kus (Univerity of Silesia, Katowice, Poland)
D. Mangelings (Free University of Brussels, Brussels, Belgium)
E. Mincsovics (Corvinus University of Budapest, Budapest, Hungary)
G. Morlock (Giessen University, Giessen, Germany)
J. Sherma (Lafayette College, Easton, PA, USA)
R. Skibiński (Medical University of Lublin, Lublin, Poland)
B. Spangenberg (Offenburg University of Applied Sciences, Germany)
T. Tuzimski (Medical University of Lublin, Lublin, Poland)
Y. Vander Heyden (Free University of Brussels, Brussels, Belgium)
A. Voelkel (Poznań University of Technology, Poznań, Poland)
B. Walczak (University of Silesia, Katowice, Poland)
W. Wasiak (Adam Mickiewicz University, Poznań, Poland)

KOWALSKA, TERESA
E-mail: kowalska@us.edu.pl

SAJEWICZ, MIECZYSLAW
E-mail:msajewic@us.edu.pl

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2020
 
Total Cites
650
WoS
Journal
Impact Factor
1,639
Rank by
Chemistry, Analytical 71/83 (Q4)
Impact Factor
 
Impact Factor
1,412
without
Journal Self Cites
5 Year
1,301
Impact Factor
Journal
0,34
Citation Indicator
 
Rank by Journal
Chemistry, Analytical 75/93 (Q4)
Citation Indicator
 
Citable
45
Items
Total
43
Articles
Total
2
Reviews
Scimago
28
H-index
Scimago
0,316
Journal Rank
Scimago
Chemistry (miscellaneous) Q3
Quartile Score
 
Scopus
393/181=2,2
Scite Score
 
Scopus
General Chemistry 215/398 (Q3)
Scite Score Rank
 
Scopus
0,560
SNIP
 
Days from
58
sumbission
 
to acceptance
 
Days from
68
acceptance
 
to publication
 
Acceptance
51%
Rate

2019  
Total Cites
WoS
495
Impact Factor 1,418
Impact Factor
without
Journal Self Cites
1,374
5 Year
Impact Factor
0,936
Immediacy
Index
0,460
Citable
Items
50
Total
Articles
50
Total
Reviews
0
Cited
Half-Life
6,2
Citing
Half-Life
8,3
Eigenfactor
Score
0,00048
Article Influence
Score
0,164
% Articles
in
Citable Items
100,00
Normalized
Eigenfactor
0,05895
Average
IF
Percentile
20,349
Scimago
H-index
26
Scimago
Journal Rank
0,255
Scopus
Scite Score
226/167=1,4
Scopus
Scite Score Rank
Chemistry (miscellaneous) 240/398 (Q3)
Scopus
SNIP
0,494
Acceptance
Rate
41%

 

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Acta Chromatographica
Language English
Size A4
Year of
Foundation
1992
Publication
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2021 Volume 33
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ISSN 2083-5736 (Online)

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