Authors:
G.-Y. Wang Key Laboratory of Chemistry of Northwestern Plant Resources and Key Laboratory for Natural Medicine of Gansu Province, Lanzhou Institute of Chemical Physics, Chinese Academy of Sciences, Lanzhou, 730000, P. R. China
School of Petroleum and Chemical Engineering, Lanzhou University of Technology, Lanzhou, 730050, P. R. China

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Y.-P. Shi Key Laboratory of Chemistry of Northwestern Plant Resources and Key Laboratory for Natural Medicine of Gansu Province, Lanzhou Institute of Chemical Physics, Chinese Academy of Sciences, Lanzhou, 730000, P. R. China

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Summary

A new method using ultra-performance liquid chromatography (UPLC) in combination with tandem mass spectrometry and a multiple reaction monitoring mode (UPLC-MS/MS-MRM) was developed for simultaneous quantitative determination of anthraquinone derivatives in Radix et Rhizoma Rhei-based medicines. A multi-mode electrospray/chemical ionization (ESCI) and negative ion mode with [M-H] and its fragments under collision-activated conditions were employed in MS/MS-MRM. The quantitative method was validated and applied to simultaneous determination of anthraquinone derivatives in 21 Radix et Rhizoma Rhei-based medicines. The limits of quantification were in the range of 3.90–9.09 ng mL−1. Average recoveries were between 95.5% and 99.8% with relative standard deviations from 1.8% to 5.3%.

  • [1]. The State Pharmacopoeia Commission of PR China 2005 Pharmacopoeia of PR China Chemical Industry Press Beijing 1718.

  • [2]. PharmaceuticalFood Safety Bureau 2006 Japanese Pharmacopoeia, Ministry of Health Labour and Welfare Tokyo 13441345.

  • [3]. European Directorate for the Quality of Medicines 2001 European Pharmacopoeia Council of Europe Strasbourg 18581859.

  • [4]. W. Jin Y.F. Wang R.L. Ge H.M. Shi C.Q. Jia P.F. Tu 2007 Rapid Commun. Mass Spectrom. 21 2351.

  • [5]. World Health Organization, WHO Monographs on Selected Medicinal Plants, Geneva, 1999, pp. 231240.

  • [6]. K.C. Huang 1993 The Pharmacology of Chinese Herbs CRC Press Boca Raton 185186.

  • [7]. J.B. Wang H.F. Li C. Jin Y. Qu X.H. Xiao 2008 J. Pharm. Biomed. Anal. 47 765.

  • [8]. The State Pharmacopoeia Commission of PR China 2010 Pharmacopoeia of PR China Chemical Industry Press Beijing 2223.

  • [9]. G.Y. Wang L.W. Xu Y.P. Shi 2011 Acta Chromatogr. 23 653.

  • [10]. G.Y. Wang H.Y. Qi Y.P. Shi 2010 J. Sep. Sci. 33 1730.

  • [11]. N.P. Singh A.P. Gupta A.K. Sinha P.S. Ahuja 2005 J. Chromatogr. A 1077 202.

  • [12]. R. Liu A. Li A. Sun 2004 J. Chromatogr. A 1052 217.

  • [13]. F.Q. Yang T.Y. Zhang G.L. Tian H.F. Cao Q.H. Liu Y. Ito 1999 J. Chromatogr. A 858 103.

  • [14]. F. Li Q.E. Cao Z. Ding 2004 Chromatograpia 59 753.

  • [15]. C.C. Lin C.I. Wu T.C. Lin J.S. Sheu 2006 J. Sep. Sci. 29 2584.

  • [16]. C.L. Liu P.L. Zhu M.C. Liu 1999 J. Chromatogr. A 857 167.

  • [17]. J. Koyama I. Morita N. Kobayashi 2007 J. Chromatogr. A 1145 183.

  • [18]. J. Stahl-Zeng V. Lange R. Ossola K. Eckhardt W. Krek R. Aebersold B. Domon 2007 Mol. Cell. Proteomics. 6 1809.

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Senior editors

Editor(s)-in-Chief: Sajewicz, Mieczyslaw, University of Silesia, Katowice, Poland

Editors(s)

  • Danica Agbaba, University of Belgrade, Belgrade, Serbia (1953-2024)
  • Łukasz Komsta, Medical University of Lublin, Lublin, Poland
  • Ivana Stanimirova-Daszykowska, University of Silesia, Katowice, Poland
  • Monika Waksmundzka-Hajnos, Medical University of Lublin, Lublin, Poland

Editorial Board

  • Ravi Bhushan, The Indian Institute of Technology, Roorkee, India
  • Jacek Bojarski, Jagiellonian University, Kraków, Poland
  • Bezhan Chankvetadze, State University of Tbilisi, Tbilisi, Georgia
  • Michał Daszykowski, University of Silesia, Katowice, Poland
  • Tadeusz H. Dzido, Medical University of Lublin, Lublin, Poland
  • Attila Felinger, University of Pécs, Pécs, Hungary
  • Kazimierz Glowniak, Medical University of Lublin, Lublin, Poland
  • Bronisław Glód, Siedlce University of Natural Sciences and Humanities, Siedlce, Poland
  • Anna Gumieniczek, Medical University of Lublin, Lublin, Poland
  • Urszula Hubicka, Jagiellonian University, Kraków, Poland
  • Krzysztof Kaczmarski, Rzeszow University of Technology, Rzeszów, Poland
  • Huba Kalász, Semmelweis University, Budapest, Hungary
  • Katarina Karljiković Rajić, University of Belgrade, Belgrade, Serbia
  • Imre Klebovich, Semmelweis University, Budapest, Hungary
  • Angelika Koch, Private Pharmacy, Hamburg, Germany
  • Piotr Kus, Univerity of Silesia, Katowice, Poland
  • Debby Mangelings, Free University of Brussels, Brussels, Belgium
  • Emil Mincsovics, Corvinus University of Budapest, Budapest, Hungary
  • Ágnes M. Móricz, Centre for Agricultural Research, Budapest, Hungary
  • Gertrud Morlock, Giessen University, Giessen, Germany
  • Anna Petruczynik, Medical University of Lublin, Lublin, Poland
  • Robert Skibiński, Medical University of Lublin, Lublin, Poland
  • Bernd Spangenberg, Offenburg University of Applied Sciences, Germany
  • Tomasz Tuzimski, Medical University of Lublin, Lublin, Poland
  • Adam Voelkel, Poznań University of Technology, Poznań, Poland
  • Beata Walczak, University of Silesia, Katowice, Poland
  • Wiesław Wasiak, Adam Mickiewicz University, Poznań, Poland
  • Igor G. Zenkevich, St. Petersburg State University, St. Petersburg, Russian Federation

 

SAJEWICZ, MIECZYSLAW
E-mail:mieczyslaw.sajewicz@us.edu.pl

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2024  
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SJR index 0.285
SJR Q rank Q3

2023  
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Journal Impact Factor 1.7
Rank by Impact Factor Q3 (Chemistry, Analytical)
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CiteScore 4.0
CiteScore rank Q2 (General Chemistry)
SNIP 0.706
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SJR index 0.344
SJR Q rank Q3

Acta Chromatographica
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Acta Chromatographica
Language English
Size A4
Year of
Foundation
1988
Volumes
per Year
1
Issues
per Year
4
Founder Institute of Chemistry, University of Silesia
Founder's
Address
PL-40-007 Katowice, Poland, Bankowa 12
Publisher Akadémiai Kiadó
Publisher's
Address
H-1117 Budapest, Hungary 1516 Budapest, PO Box 245.
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Publisher
Chief Executive Officer, Akadémiai Kiadó
ISSN 2083-5736 (Online)

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