Authors:
,
, and
T. Tomsej
T. Tomsej
Institute of Clean Technologies, VŠB-Technical University of Ostrava, 17. listopadu 15, 708 33, Ostrava-Poruba, Czech Republic
Search for other papers by T. Tomsej in
Current site
Google Scholar
PubMed
Search for other papers by T. Tomsej in
Current site
Google Scholar
PubMed
S. Tomsejova
S. Tomsejova
Institute of Public Health Ostrava, National Reference Laboratory for POP, Partyzanske namesti 7, 702 00, Ostrava, Czech Republic
Search for other papers by S. Tomsejova in
Current site
Google Scholar
PubMed
Search for other papers by S. Tomsejova in
Current site
Google Scholar
PubMed
V. Dombek
V. Dombek
Institute of Clean Technologies, VŠB-Technical University of Ostrava, 17. listopadu 15, 708 33, Ostrava-Poruba, Czech Republic
Search for other papers by V. Dombek in
Current site
Google Scholar
PubMed
Search for other papers by V. Dombek in
Current site
Google Scholar
PubMed
Summary
Effect of column bleed on trueness of determination of trace levels of dibenzofuranes (PCDD/F) and biphenyls (PCB) by gas chromatography-high-resolution mass spectrometry (GC-HRMS) was studied. As a result of extensive bleed of an arylenesiloxane capillary column, fluctuations of abundance ratios of monitored ions were observed, making exact determination of target analytes impossible. These effects were observed on food samples as well as on pure standard mixtures. The column bleed affected the abundance ratios of PCDD/F and PCB within the range of 13–328 pg of target analyte/mL, and higher levels of analytes remained intact. An analysis of diluted calibration mixtures is recommended as a tool for detection of column bleed.
ProCite
RefWorks
Reference Manager
BibTeX
Zotero
EndNote
-
[1]. EPA Method 1613, Revision B: Tetra-through Octa-chlorinated Dioxins and Furans by Isotope Dilution HRGC/HRMS, US Environmental Protection Agency, Engineering and Analysis Division, 1994.
-
[2]. Compendium Method 9A: Determination of Polychlorinated, Polybrominated and Brominated/Chlorinated Dibenzo-p-Dioxins and Dibenzofurans in Ambient Air, Compendium of Methods for the Determination of Toxic Organic Compounds in Ambient Air, US Environmental Protection Agency, Center for Environmental Research Information, 1999.
-
[3]. EN 1948–3 Stationary Source Emissions. Determination of the Mass Concentration of PCDDs/PCDFs and Dioxin-Like PCBs, 2006.
-
[4]. EN 16215 Animal Feeding Stuff — Determination of Dioxins and Dioxin-Like PCB by GC/HRMS and of Indicator PCBs by GC/HRMS, 2012.
-
[5]. Method 1614A Brominated Diphenyl Ethers in Water, Soil, Sediment, and Tissue by HRGC/HRMS, US Environmental Protection Agency, Engineering and Analysis Division, 2010.
-
[6]. Method 1699: Pesticides in Water, Soil, Sediment, Biosolids, and Tissue by HRGC/HRMS, US Environmental Protection Agency, Engineering and Analysis Division, 2007.
-
[7]. K. Grob G. Grob 1982 J. HRC & CC 5 349.
-
[8]. S. Hoffmann L.G. Blomberg J. Buijten K. Markides T. Wännman 1984 J. Chromatogr. 302 95.
-
[9]. B. S. Middleditch , Analytical Artifacts: GC, MS, HPLC, TLC and PC, Elsevier, 1989, pp. 165–168.
-
[10]. L.G. Blomberg 2001 LC-GC Europe 142 106.
-
[11]. J. Buijten L. Blomberg S. Hoffmann K. Markides T. Wännman 1984 J. Chromatogr. 301 265.
-
[12]. A. Bermgard L. Blomberg 1987 J. HRC & CC 10 302.
-
[13]. D. Rood 1995 A Practical Guide to the Care, Maintenance, and Troubleshooting of Capillary Gas Chromatographic Systems 2nd edn Hüthig GmbH Heidelberg 57.
-
[14]. J. de Zeeuw J. Luong 2002 Trends Anal. Chem. 21 9–10 594.
-
[15]. J. De Zeeuw L. Joziasse J. Peen P. Heijnsdijk D. Zwiep 2003 Am. Lab. (Shelton, CT, U. S.) 35 16 30.
-
[16]. M. Thompson S.L.R. Ellison R. Wood 2006 Pure Appl. Chem. 78 145.
Senior editors
Editor(s)-in-Chief: Sajewicz, Mieczyslaw, University of Silesia, Katowice, Poland
Editors(s)
- Danica Agbaba, University of Belgrade, Belgrade, Serbia (1953-2024)
- Łukasz Komsta, Medical University of Lublin, Lublin, Poland
- Ivana Stanimirova-Daszykowska, University of Silesia, Katowice, Poland
- Monika Waksmundzka-Hajnos, Medical University of Lublin, Lublin, Poland
Editorial Board
- Ravi Bhushan, The Indian Institute of Technology, Roorkee, India
- Jacek Bojarski, Jagiellonian University, Kraków, Poland
- Bezhan Chankvetadze, State University of Tbilisi, Tbilisi, Georgia
- Michał Daszykowski, University of Silesia, Katowice, Poland
- Tadeusz H. Dzido, Medical University of Lublin, Lublin, Poland
- Attila Felinger, University of Pécs, Pécs, Hungary
- Kazimierz Glowniak, Medical University of Lublin, Lublin, Poland
- Bronisław Glód, Siedlce University of Natural Sciences and Humanities, Siedlce, Poland
- Anna Gumieniczek, Medical University of Lublin, Lublin, Poland
- Urszula Hubicka, Jagiellonian University, Kraków, Poland
- Krzysztof Kaczmarski, Rzeszow University of Technology, Rzeszów, Poland
- Huba Kalász, Semmelweis University, Budapest, Hungary
- Katarina Karljiković Rajić, University of Belgrade, Belgrade, Serbia
- Imre Klebovich, Semmelweis University, Budapest, Hungary
- Angelika Koch, Private Pharmacy, Hamburg, Germany
- Piotr Kus, Univerity of Silesia, Katowice, Poland
- Debby Mangelings, Free University of Brussels, Brussels, Belgium
- Emil Mincsovics, Corvinus University of Budapest, Budapest, Hungary
- Ágnes M. Móricz, Centre for Agricultural Research, Budapest, Hungary
- Gertrud Morlock, Giessen University, Giessen, Germany
- Anna Petruczynik, Medical University of Lublin, Lublin, Poland
- Robert Skibiński, Medical University of Lublin, Lublin, Poland
- Bernd Spangenberg, Offenburg University of Applied Sciences, Germany
- Tomasz Tuzimski, Medical University of Lublin, Lublin, Poland
- Adam Voelkel, Poznań University of Technology, Poznań, Poland
- Beata Walczak, University of Silesia, Katowice, Poland
- Wiesław Wasiak, Adam Mickiewicz University, Poznań, Poland
- Igor G. Zenkevich, St. Petersburg State University, St. Petersburg, Russian Federation
SAJEWICZ, MIECZYSLAW
E-mail:mieczyslaw.sajewicz@us.edu.pl
Indexing and Abstracting Services:
- Science Citation Index
- SCOPUS
- DOAJ
- Sci Search
- Research Alert
- Chemistry Citation Index and Current Content/Physical
- Chemical and Earth Sciences
- GoogleScholar
- Index Copernicus
- CABI
- CABELLS Journalytics
| 2024 | |
|---|---|
| Scopus | |
| CiteScore | |
| CiteScore rank | |
| SNIP | |
| Scimago | |
| SJR index | 0.285 |
| SJR Q rank | Q3 |
| 2023 | |
|---|---|
| Web of Science | |
| Journal Impact Factor | 1.7 |
| Rank by Impact Factor | Q3 (Chemistry, Analytical) |
| Journal Citation Indicator | 0.43 |
| Scopus | |
| CiteScore | 4.0 |
| CiteScore rank | Q2 (General Chemistry) |
| SNIP | 0.706 |
| Scimago | |
| SJR index | 0.344 |
| SJR Q rank | Q3 |
| Acta Chromatographica | |
|---|---|
| Publication Model | Online only Gold Open Access |
| Submission Fee | none |
| Article Processing Charge |
700 EUR/article For MS submitted before 1 Feb 2025: 400 EUR/article |
| Regional discounts on country of the funding agency | World Bank Lower-middle-income economies: 50% World Bank Low-income economies: 100% |
| Further Discounts | Editorial Board / Advisory Board members: 50% Corresponding authors, affiliated to an EISZ member institution subscribing to the journal package of Akadémiai Kiadó: 100% |
| Subscription Information | Gold Open Access |
| Purchase per Title | |
| Acta Chromatographica | |
|---|---|
| Language | English |
| Size | A4 |
| Year of Foundation |
1988 |
| Volumes per Year |
1 |
| Issues per Year |
4 |
| Founder | Institute of Chemistry, University of Silesia |
| Founder's Address |
PL-40-007 Katowice, Poland, Bankowa 12 |
| Publisher | Akadémiai Kiadó |
| Publisher's Address |
H-1117 Budapest, Hungary 1516 Budapest, PO Box 245. |
| Responsible Publisher |
Chief Executive Officer, Akadémiai Kiadó |
| ISSN | 2083-5736 (Online) |
Monthly Content Usage
| Abstract Views | Full Text Views | PDF Downloads | |
|---|---|---|---|
| Jan 2025 | 0 | 38 | 3 |
| Feb 2025 | 0 | 42 | 5 |
| Mar 2025 | 0 | 50 | 4 |
| Apr 2025 | 0 | 13 | 2 |
| May 2025 | 0 | 12 | 2 |
| Jun 2025 | 0 | 14 | 1 |
| Jul 2025 | 0 | 0 | 0 |
Authors:
, , , , , , and
Authors:
, , , , , , and
Copyright Akadémiai Kiadó AKJournals is the trademark of Akadémiai Kiadó's journal publishing business branch.
Powered by PubFactory