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J. Wang Sun Yat-sen University, Guangzhou 510275, PR China

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M. Liu Sun Yat-sen University, Guangzhou 510275, PR China

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X. Tong Sun Yat-sen University, Guangzhou 510275, PR China

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W. Peng Sun Yat-sen University, Guangzhou 510275, PR China

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H. Cao National Engineering Research Center for Modernization of Traditional Chinese Medicine, , Zhuhai 519020, PR China

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W. Su Sun Yat-sen University, Guangzhou 510275, PR China

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Shenqi Fuzheng Injection (SFI) is a traditional Chinese medicine injection, widely used to enhance immune function of clinical cancer patients undergoing chemotherapy. In this study, a high-performance liquid chromatography-diode array detection-evaporative light scattering detection (HPLC-DAD-ELSD) method was established for quality control of SFI, which could simultaneously semiquantitatively reflect the constituents displayed in the chromatographic profile of SFI. The relative retention time and relative peak areas of the 21 common peaks related to the reference peak were calculated. The validity and advantage of this method were validated by systematically comparing chromatograms of 10 batches of SFI samples with the analytical methods of principal component analysis and angle cosine method recommended by the State Food and Drug Administration of China. Moreover, a total of 21 constituents of SFI were identified or tentatively characterized in the fingerprint via ultrafast liquid chromatography-diode array detection-quadrupole time-of-flight (UFLC-DAD-Q-TOF) tandem mass spectrometry technique on the basis of the retention time, ultraviolet spectra, fragmentation patterns, and reported literatures. All the results proved that the technique was useful in comprehensive quality evaluation of SFI and further study.

  • [1]

    Z.J. Dai , X.J. Wan, H.F. Kang, Z.Z. Ji, L. Liu, X.X. Liu, L.Q. Song, W.L. Min, and X.B. Ma, J. Tradit. Chin. Med., 28, 3438 (2008)

  • [2]

    X.Y. Zhu , X.Z. Zhang, and X.Y. Zhong, Chin. J. Integr. Tradit. West. Med., 30, 205207 (2010)

  • [3]

    Y. Bo , H.S. Li, Y.C. Qi, and M.Y. Lu, Chin. J. Integr. Med., 13, 3740 (2007)

  • [4]

    J.X. Wang , X. Tong, P.B. Li, H. Cao, and W.W. Su, J. Ethnopharmacol., 139, 788795 (2012)

  • [5]

    Y.Z. Liang , P. Xie, and K. Chan, J. Chromatogr. B: Analy. Technol. Biomed. Life Sci., 812, 5370 (2004)

  • [6]

    P. Drašar and J. Moravcova, J. Chromatogr. B: Analy. Technol. Biomed. Life Sci., 812, 321 (2004)

  • [7]

    P.S. Xie , S.B. Chen, Y.Z. Liang, X.H. Wang, R.T. Tian, and R. Upton, J. Chromatogr. A, 1112, 171180 (2006)

  • [8]

    M. Cuendet , O. Potterat, and K. Hostettmann, Phytochemistry, 56, 631636 (2001)

  • [9]

    C.Y. Li , H.X. Xu, Q.B. Han, and T.S. Wu, J. Chromatogr. A, 1216, 21242129 (2009)

  • [10]

    X.F. Ma , P.F. Tu, Y.J. Chen, T.Y. Zhang, Y. Wei, and Y.C. Ito, J. Chromatogr. A, 1023, 311315 (2004)

  • [11]

    C.F. Qiao , Z.D. He, Q.B. Han, H.X. Xu, R.W. Jiang, S.L. Li, Y.B. Zhang, P.P.H. But, and P.C. Shaw, J. Food Drug Anal., 15, 258264 (2007)

  • [12]

    X.Q. Ma , Q. Shi, J.A. Duan, T.T.X. Dong, and K.W.K. Tsim, J. Agric. Food Chem., 50, 48614866 (2002)

  • [13]

    M.H. Liu , X. Tong, J.X. Wang, W. Zou, H. Cao, and W.W. Su, J. Pharm. Biomed., 74, 141155 (2013)

  • [14]

    W.L. Li , Y.Y. Yu, J. Zhao, X.D. Wang, Z.T. Hu, and D. Xu, Chin. Pharm. J., 43, 968–970+1032 (2008)

  • [15]

    J. Li , T. Chen, Y. Wang, J.J. Song, Z.P. Ma, and M. Meng, Chin. Tradit. Herb. Drugs, 40, 804806 (2009)

  • [16]

    J. Kang , L. Zhou, J. Sun, J. Han, and D.A. Guo, J. Pharm. Biomed., 47, 778785 (2008)

  • [17]

    L.F. Huang , M.J. Wu, X.J. Sun, F.Q. Guo, Y.Z. Liang, and X.R. Li, J. Cent. South Univ. Technol., 11, 295299 (2004)

  • [18]

    P. Liu , Y.Y. Li, H.M. Li, D.J. Wan, and Y.J. Tang, Anal. Chim. Acta, 687, 159167 (2011)

  • [19]

    V. Gokmen and J. Acar, J. Chromatogr. A, 847, 6974 (1999)

  • [20]

    I.G. Zenkevich , A.I. Pimenov, L.I. Sokolova, and V.G. Makarov, Russ. J. Appl. Chem., 74, 11641168 (2001)

  • [21]

    X.D. Wen , L.W. Qi, P. Li, K.D. Bao, X.W. Yan, L. Yi, and C.Y. Li, J. Chromatogr. B: Anal. Technol. Biomed. Life Sci., 865, 99105 (2008)

  • [22]

    J.Y. Zhang , G.D. Yang, R. Lin, and Z. Hu, Biomed. Chromatogr., 25, 450457 (2011)

  • [23]

    D. Song , X.M. Cheng, L.Y. Li, G.Y. Zhong, and Z.T. Wang, Chin. J. Chin. Mater. Med., 33, 21332135 (2008)

  • [24]

    J. Zhao , Q.T. Yu, P. Li, P. Zhou, Y.J. Zhang, and W. Wang, J. Sep. Sci., 31, 255261 (2008)

  • [25]

    C. Chu , L.W. Qi, B. Li, W. Gao, and P. Li, Curr. Org. Chem., 14, 17921807 (2010)

  • [26]

    D. Wang , Y. Song, S.L. Li, Y.Y. Bian, J. Guan, and P. Li, J. Sep. Sci., 29, 20122022 (2006)

  • [27]

    S.S. Jensen , X. Ariza, P. Nielsen, J. Vilarrasa, and F. Kirpekar, J. Mass. Spectrom., 42, 4957 (2007)

  • [28]

    A. Bond , E. Dudley, F. Lemiere, R. Tuytten, S. El-Sharkawi, A.G. Brenton, E.L. Esmans, and R.P. Newton, Rapid Commun. Mass Spectrom., 20, 137150 (2006)

    • Search Google Scholar
    • Export Citation
  • [29]

    E.L. Zins , S. Rochut, and C. Pepe, J. Mass Spectrom., 44, 813820 (2009)

  • [30]

    M. Imhoff , Z.W. Deng, and M.A. Huels, Int. J. Mass Spectrom., 262, 154160 (2007)

  • [31]

    I. Manet , L. Francini, S. Masiero, S. Pieraccini, G.P. Spada, and G. Gottarelli, Helv. Chim. Acta, 84, 20962107 (2001)

  • [32]

    S. Hann , A. Zenker, M. Galanski, T.L. Bereuter, G. Stingeder, and B.K. Keppler, Fresenius' J. Anal. Chem., 370, 581586 (2001)

  • [33]

    K. Hanhineva , P. Soininen, M.J. Anttonen, H. Kokko, I. Rogachev, A. Aharoni, R. Laatikainen, and S. Karenlampi, Phytochem. Analysis, 20, 353364 (2009)

    • Search Google Scholar
    • Export Citation
  • [34]

    D. Song , G.X. Chou, G.Y. Zhong, and Z.T. Wang, Helv. Chim. Acta, 91, 19841988 (2008)

  • [35]

    C.F. Qiao , Z.D. He, Q.B. Han, J.Z. Song, and H.X. Xu, Chin. J. Chin. Mater. Med., 31, 744746 (2006)

  • [36]

    L.W. Qi , Q.T. Yu, L. Yi, M.T. Ren, X.D. Wen, Y.X. Wang, and P. Li, J. Sep. Sci., 31, 97106 (2008)

  • [37]

    S.P. Singh, Wahajuddin , M.M. Ali, and G.K. Jain, J. Sep. Sci., 33, 33263334 (2010)

  • [38]

    S.P. Singh, Wahajuddin , M.M. Ali, K. Kohli, and G.K. Jain, J. Chromatogr. B: Anal. Technol. Biomed. Life Sci., 879, 28452851 (2011)

  • [39]

    L.W. Qi , X.D. Wen, J. Cao, C.Y. Li, P. Li, L. Yi, Y.X. Wang, X.L. Cheng, and X.X. Ge, Rapid Commun. Mass Spectrom., 22, 24932509 (2008)

  • [40]

    T. Xie , Y. Liang, H.P. Hao, J.Y. A, L. Xie, P. Gong, C. Dai, L.S. Liu, A. Kang, X. Zheng, and G.J. Wang, J. Chromatogr. A, 1227, 234244 (2012)

    • Search Google Scholar
    • Export Citation
  • [41]

    C. Chu , H.X. Cai, M.T. Ren, E.H. Liu, B. Li, L.W. Qi, and P. Li, J. Sep. Sci., 33, 570581 (2010)

  • [42]

    H.J. Kwon , Y.D. Park, J. Chromatogr. A, 1232, 212217 (2012)

  • [43]

    Y.G. Zu , M.M. Yan, Y.J. Fu, W. Liu, L. Zhang, C.B. Gu, and T. Efferth, J. Sep. Sci., 32, 517525 (2009)

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Senior editors

Editor(s)-in-Chief: Kowalska, Teresa (1946-2023)

Editor(s)-in-Chief: Sajewicz, Mieczyslaw, University of Silesia, Katowice, Poland

Editors(s)

  • Danica Agbaba, University of Belgrade, Belgrade, Serbia
  • Łukasz Komsta, Medical University of Lublin, Lublin, Poland
  • Ivana Stanimirova-Daszykowska, University of Silesia, Katowice, Poland
  • Monika Waksmundzka-Hajnos, Medical University of Lublin, Lublin, Poland

Editorial Board

  • Ravi Bhushan, The Indian Institute of Technology, Roorkee, India
  • Jacek Bojarski, Jagiellonian University, Kraków, Poland
  • Bezhan Chankvetadze, State University of Tbilisi, Tbilisi, Georgia
  • Michał Daszykowski, University of Silesia, Katowice, Poland
  • Tadeusz H. Dzido, Medical University of Lublin, Lublin, Poland
  • Attila Felinger, University of Pécs, Pécs, Hungary
  • Kazimierz Glowniak, Medical University of Lublin, Lublin, Poland
  • Bronisław Glód, Siedlce University of Natural Sciences and Humanities, Siedlce, Poland
  • Anna Gumieniczek, Medical University of Lublin, Lublin, Poland
  • Urszula Hubicka, Jagiellonian University, Kraków, Poland
  • Krzysztof Kaczmarski, Rzeszow University of Technology, Rzeszów, Poland
  • Huba Kalász, Semmelweis University, Budapest, Hungary
  • Katarina Karljiković Rajić, University of Belgrade, Belgrade, Serbia
  • Imre Klebovich, Semmelweis University, Budapest, Hungary
  • Angelika Koch, Private Pharmacy, Hamburg, Germany
  • Piotr Kus, Univerity of Silesia, Katowice, Poland
  • Debby Mangelings, Free University of Brussels, Brussels, Belgium
  • Emil Mincsovics, Corvinus University of Budapest, Budapest, Hungary
  • Ágnes M. Móricz, Centre for Agricultural Research, Budapest, Hungary
  • Gertrud Morlock, Giessen University, Giessen, Germany
  • Anna Petruczynik, Medical University of Lublin, Lublin, Poland
  • Robert Skibiński, Medical University of Lublin, Lublin, Poland
  • Bernd Spangenberg, Offenburg University of Applied Sciences, Germany
  • Tomasz Tuzimski, Medical University of Lublin, Lublin, Poland
  • Yvan Vander Heyden, Free University of Brussels, Brussels, Belgium
  • Adam Voelkel, Poznań University of Technology, Poznań, Poland
  • Brata Walczak, University of Silesia, Katowice, Poland
  • Wiesław Wasiak, Adam Mickiewicz University, Poznań, Poland
  • Igor G. Zenkevich, St. Petersburg State University, St. Petersburg, Russian Federation

 

KOWALSKA, TERESA (1946-2023)
E-mail: kowalska@us.edu.pl

SAJEWICZ, MIECZYSLAW
E-mail:msajewic@us.edu.pl

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2023  
Web of Science  
Journal Impact Factor 1.7
Rank by Impact Factor Q3 (Chemistry, Analytical)
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CiteScore 4.0
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Acta Chromatographica
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Acta Chromatographica
Language English
Size A4
Year of
Foundation
1988
Volumes
per Year
1
Issues
per Year
4
Founder Institute of Chemistry, University of Silesia
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Address
PL-40-007 Katowice, Poland, Bankowa 12
Publisher Akadémiai Kiadó
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ISSN 2083-5736 (Online)

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