Acta Chromatographica
Volume/Issue:
Volume 28: Issue 1
Simultaneous determination of four major constituents in Citri Grandis Exocarpium by HPLC-DAD
Authors:
X.X. Yu Sun Yat-Sen University, No. 132 East Waihuan Rd., Guangzhou Higher Education Mega Center, Guangzhou, 510006, China
Guangdong Technology Research Center for Advanced Chinese Medicine, Guangzhou 510006, China

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Q.D. Liu Sun Yat-Sen University, No. 132 East Waihuan Rd., Guangzhou Higher Education Mega Center, Guangzhou, 510006, China
Guangdong Technology Research Center for Advanced Chinese Medicine, Guangzhou 510006, China

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J.W. Wu Sun Yat-Sen University, No. 132 East Waihuan Rd., Guangzhou Higher Education Mega Center, Guangzhou, 510006, China
Guangdong Technology Research Center for Advanced Chinese Medicine, Guangzhou 510006, China

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Z.K. Liang Sun Yat-Sen University, No. 132 East Waihuan Rd., Guangzhou Higher Education Mega Center, Guangzhou, 510006, China
Guangdong Technology Research Center for Advanced Chinese Medicine, Guangzhou 510006, China

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M.Q. Zhao Sun Yat-Sen University, No. 132 East Waihuan Rd., Guangzhou Higher Education Mega Center, Guangzhou, 510006, China
Guangdong Technology Research Center for Advanced Chinese Medicine, Guangzhou 510006, China

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X.J. Xu Sun Yat-Sen University, No. 132 East Waihuan Rd., Guangzhou Higher Education Mega Center, Guangzhou, 510006, China
Guangdong Technology Research Center for Advanced Chinese Medicine, Guangzhou 510006, China

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Pages:
129–143
Online Publication Date:
Mar 2016
Publication Date:
01 Mar 2016
Article Category:
Research Article
DOI:
https://doi.org/10.1556/1326.2016.28.1.10
Keywords:
determination; Citri Grandis Exocarpium; HPLC-DAD
Open access

Citri Grandis Exocarpium (CGE) is a traditional Chinese medicine with a variety of biological activities. For efficient quality control of CGE, a simple, rapid, and accurate high-performance liquid chromatographic (HPLC) method was developed for simultaneous determination of four main compounds (naringin, rhoifolin, meranzin hydrate, and isoimperatorin) in this herb. These four compounds were separated on a C18 column by gradient elution with methanol and water. The flow rate was 1.0 mL·min−1, and the detection wavelength was 324 nm. The recoveries of the method ranged from 96.32% to 103.71%, and good linear relationships (r2 > 0.9998) over relative wide concentration ranges were obtained. Then this validated method was successfully applied to the analysis of nine batches of CGE samples.

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Cover Acta Chromatographica
Acta Chromatographica
Online ISSN:
2083-5736
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Senior editors

Editor(s)-in-Chief: Kowalska, Teresa (1946-2023)

Editor(s)-in-Chief: Sajewicz, Mieczyslaw, University of Silesia, Katowice, Poland

Editors(s)

  • Danica Agbaba, University of Belgrade, Belgrade, Serbia
  • Łukasz Komsta, Medical University of Lublin, Lublin, Poland
  • Ivana Stanimirova-Daszykowska, University of Silesia, Katowice, Poland
  • Monika Waksmundzka-Hajnos, Medical University of Lublin, Lublin, Poland

Editorial Board

  • Ravi Bhushan, The Indian Institute of Technology, Roorkee, India
  • Jacek Bojarski, Jagiellonian University, Kraków, Poland
  • Bezhan Chankvetadze, State University of Tbilisi, Tbilisi, Georgia
  • Michał Daszykowski, University of Silesia, Katowice, Poland
  • Tadeusz H. Dzido, Medical University of Lublin, Lublin, Poland
  • Attila Felinger, University of Pécs, Pécs, Hungary
  • Kazimierz Glowniak, Medical University of Lublin, Lublin, Poland
  • Bronisław Glód, Siedlce University of Natural Sciences and Humanities, Siedlce, Poland
  • Anna Gumieniczek, Medical University of Lublin, Lublin, Poland
  • Urszula Hubicka, Jagiellonian University, Kraków, Poland
  • Krzysztof Kaczmarski, Rzeszow University of Technology, Rzeszów, Poland
  • Huba Kalász, Semmelweis University, Budapest, Hungary
  • Katarina Karljiković Rajić, University of Belgrade, Belgrade, Serbia
  • Imre Klebovich, Semmelweis University, Budapest, Hungary
  • Angelika Koch, Private Pharmacy, Hamburg, Germany
  • Piotr Kus, Univerity of Silesia, Katowice, Poland
  • Debby Mangelings, Free University of Brussels, Brussels, Belgium
  • Emil Mincsovics, Corvinus University of Budapest, Budapest, Hungary
  • Ágnes M. Móricz, Centre for Agricultural Research, Budapest, Hungary
  • Gertrud Morlock, Giessen University, Giessen, Germany
  • Anna Petruczynik, Medical University of Lublin, Lublin, Poland
  • Robert Skibiński, Medical University of Lublin, Lublin, Poland
  • Bernd Spangenberg, Offenburg University of Applied Sciences, Germany
  • Tomasz Tuzimski, Medical University of Lublin, Lublin, Poland
  • Yvan Vander Heyden, Free University of Brussels, Brussels, Belgium
  • Adam Voelkel, Poznań University of Technology, Poznań, Poland
  • Brata Walczak, University of Silesia, Katowice, Poland
  • Wiesław Wasiak, Adam Mickiewicz University, Poznań, Poland
  • Igor G. Zenkevich, St. Petersburg State University, St. Petersburg, Russian Federation

 

KOWALSKA, TERESA (1946-2023)
E-mail: kowalska@us.edu.pl

SAJEWICZ, MIECZYSLAW
E-mail:msajewic@us.edu.pl

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Acta Chromatographica
Language English
Size A4
Year of
Foundation		 1988
Volumes
per Year		 1
Issues
per Year		 4
Founder Institute of Chemistry, University of Silesia
Founder's
Address		 PL-40-007 Katowice, Poland, Bankowa 12
Publisher Akadémiai Kiadó
Publisher's
Address		 H-1117 Budapest, Hungary 1516 Budapest, PO Box 245.
Responsible
Publisher		 Chief Executive Officer, Akadémiai Kiadó
ISSN 2083-5736 (Online)

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