JPC - Journal of Planar Chromatography - Modern TLC
Volume/Issue:
Volume 18: Issue 104
Application of densitometry and spectrophotometry for determination of gallic acid in tea after chromatographic separation
Authors:
Urszula Hachuła Silesian University Institute of Chemistry, Department of Analytical Chemistry 9 Szkolna Street 40-006 Katowice Poland

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Sabina Anikiel Silesian University Institute of Chemistry, Department of Analytical Chemistry 9 Szkolna Street 40-006 Katowice Poland

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Mieczysław Sajewicz Silesian University Institute of Chemistry, Department of Analytical Chemistry 9 Szkolna Street 40-006 Katowice Poland

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Pages:
290–293
Online Publication Date:
17 Mar 2007
Publication Date:
01 Aug 2005
Article Category:
Research Article
DOI:
https://doi.org/10.1556/jpc.18.2005.4.7
Keywords:
Gallic acid; TLC separation; Determination; Densitometry; Spectrophotometry; Tea
Restricted access

Tea is one of the most popular beverages in the world. The exact composition of tea depends on the manufacturing process. Our goal was to optimize the chromatographic conditions for separation of tea extract and to apply the optimized method for determination of gallic acid in oolong, black, and pu-erh tea. Chromatographic separation was performed on silica gel 60 F 254 TLC plates with chloroform-ethyl acetate-formic acid, 5 + 4 + 1 ( v/v ), as mobile phase. Densitometric measurement was performed in the ultraviolet region at λ = 280 nm. Quantification of gallic acid in pu-erh tea was also performed by a spectrophotometric method based on the coupled redox complexation reaction occurring in the system Fe(III)-gallic acid-2,2′-dipyridyl ( λmax = 522 nm).

  • I. Tutakowska and P. Małecki , Herbata — napój dla ciała i ducha, Media Publication, 2000.

  • I. Nartowska and M. Wasek , Farm. Pol. 20 (58) (2002) 965–971.

    Wasek M. , '' (2002 ) 20 Farm. Pol. : 965 -971 .

  • S. Kohlmünzer , Farmakognozja, Wydawnictwo Lekarskie PZWL, Warszawa, 1998.

    Kohlmünzer S. , '', in Farmakognozja , (1998 ) -.

  • J.J. Dallug and B.C. Nelson , J. Chromatogr. A 881 (2000) 441–424.

    Nelson B.C. , '' (2000 ) 881 J. Chromatogr. A : 441 -424 .

  • D.J. Zeeb, B.C. Nelson, K. Albert , and J.J. Dalluge , Anal. Chem. 72 (2000) 5020–5026.

    Dalluge J.J. , '' (2000 ) 72 Anal. Chem. : 5020 -5026 .

  • Y.S. Lin, Y.J. Tsai, Y.S. Tsay , and J.K. Lin , J. Agric. Food Chem. 51 (2003) 1864–1873.

    Lin J.K. , '' (2003 ) 51 J. Agric. Food Chem. : 1864 -1873 .

  • S. Khokha and S.G.M. Magnusdottir , J. Agric. Food Chem. 50 (2000) 565–570.

    Magnusdottir S.G.M. , '' (2000 ) 50 J. Agric. Food Chem. : 565 -570 .

  • P. Valera, F. Pablos , and A.G. Gonzalez , Talanta 43 (1996) 415–419.

    Gonzalez A.G. , '' (1996 ) 43 Talanta : 415 -419 .

  • J.P. Aucamp, Y. Har , and Z. Apostolides , J. Chromatogr. A 876 (2000) 235–242.

    Apostolides Z. , '' (2000 ) 876 J. Chromatogr. A : 235 -242 .

  • Y. Zuo, H. Che , and Y. Deng , Talanta 57 (2002) 307–316.

    Deng Y. , '' (2002 ) 57 Talanta : 307 -316 .

  • Y. Amakura, M. Okada, S. Tsuji , and Y. Tonogai , J. Chromatogr. A 891 (2000) 183–188.

    Tonogai Y. , '' (2000 ) 891 J. Chromatogr. A : 183 -188 .

  • S.D. Dmitrienko, O.M. Medvedeva, A.A. Ivanov, O.A. Shpigun , and Yu.A. Zolotov , Anal. Chim. Acta 469 (2002) 295–299.

    Zolotov Yu.A. , '' (2002 ) 469 Anal. Chim. Acta : 295 -299 .

  • B.L. Lee and C.N. Ong , J. Chromatogr. A 881 (2000) 439–447.

    Ong C.N. , '' (2000 ) 881 J. Chromatogr. A : 439 -447 .

  • H. Horie and K. Kohata , J. Chromatogr. A 881 (2000) 425.

    Kohata K. , '' (2000 ) 881 J. Chromatogr. A : 425 -.

  • T. Goto, Y. Yoshida, M. Kiso , and H. Nagashima , J. Chromatogr. A 749 (1996) 295–299.

    Nagashima H. , '' (1996 ) 749 J. Chromatogr. A : 295 -299 .

  • J.K. Lin, C.L. Lin, Y.C. Lian, S.Y.L. Shiau , and I.M. Juan , J. Agric. Food Chem. 46 (1998) 3635–3642.

    Juan I.M. , '' (1998 ) 46 J. Agric. Food Chem. : 3635 -3642 .

  • P. Stremple , J. High Resol. Chromatogr. 19 (1996) 581.

    Stremple P. , '' (1996 ) 19 J. High Resol. Chromatogr. : 581 -.

  • D.L. Luthria, A.D. Jones, A.L. Donovan , and J. Waterhouse , J. High Resol. Chromatogr. 20 (1997) 621.

    Waterhouse J. , '' (1997 ) 20 J. High Resol. Chromatogr. : 621 -.

  • R. Amarowicz and F. Shahidi , Food Res. Int. 29 (1996) 71.

    Shahidi F. , '' (1996 ) 29 Food Res. Int. : 71 -.

  • M. Zhu and P. G. Xiao , Phytother. Res. Int. 5 (1991) 239.

    Xiao P. G. , '' (1991 ) 5 Phytother. Res. Int. : 239 -.

  • H.P. Singh, S.D. Ravindranath , and C. Singh , J. Agric. Food Chem. 47 (1999) 1041.

    Singh C. , '' (1999 ) 47 J. Agric. Food Chem. : 1041 -.

  • A.A.G. Kivits, F.J.P. van der Sman , and L.B.M. Tijburg , Int. J. Food Sci. Nutr. 48 (1997) 387.

    Tijburg L.B.M. , '' (1997 ) 48 Int. J. Food Sci. Nutr. : 387 -.

  • H. Schultz, U.H. Engelhardt, A. Wegent, H.H. Drews , and S. Lapczyński , J. Agric. Food Chem. 47 (1999) 5064.

    Lapczyński S. , '' (1999 ) 47 J. Agric. Food Chem. : 5064 -.

  • U. Hachuła, S. Anikiel , and M. Połowniak , J. Planar Chromatogr. 17 (2004) 51–53.

    Połowniak M. , '' (2004 ) 17 J. Planar Chromatogr. : 51 -53 .
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Cover JPC - Journal of Planar Chromatography - Modern TLC
JPC - Journal of Planar Chromatography - Modern TLC
Print ISSN:
0933-4173
Online ISSN:
1789-0993

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Manuscript Submission: HERE

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Journal of Planar Chromatography - Modern TLC
Language English
Size A4
Year of
Foundation		 1988
Volumes
per Year		 1
Issues
per Year		 6
Founder Akadémiai Kiadó
Founder's
Address		 H-1117 Budapest, Hungary 1516 Budapest, PO Box 245.
Publisher Akadémiai Kiadó
Springer Nature Switzerland AG
Publisher's
Address		 H-1117 Budapest, Hungary 1516 Budapest, PO Box 245.
CH-6330 Cham, Switzerland Gewerbestrasse 11.
Responsible
Publisher		 Chief Executive Officer, Akadémiai Kiadó
ISSN 0933-4173 (Print)
ISSN 1789-0993 (Online)

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