JPC - Journal of Planar Chromatography - Modern TLC
Volume/Issue:
Volume 27: Issue 2
Optimization Condition for Thin-Layer Identification of Bronzes after Anodic Sampling
Authors:
Danijela AšpergerFaculty of Chemical Engineering and Technology Department of Analytical Chemistry Marulićev trg 20 HR-10000 Zagreb Croatia

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Lidija ĆurkovićFaculty of Mechanical Engineering and Naval Architecture Department of Materials Ivana Lučića 5 HR-10000 Zagreb Croatia

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Alka HorvatFaculty of Chemical Engineering and Technology Department of Analytical Chemistry Marulićev trg 20 HR-10000 Zagreb Croatia

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Marija Kaštelan-MacanFaculty of Chemical Engineering and Technology Department of Analytical Chemistry Marulićev trg 20 HR-10000 Zagreb Croatia

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Pages:
84–87
Online Publication Date:
14 Mar 2014
Publication Date:
01 Apr 2014
Article Category:
Research Article
DOI:
https://doi.org/10.1556/jpc.27.2014.2.2
Keywords:
Cu-alloy; Anodic sampling; Identification of metal ions; Thin-layer chromatography
Restricted access

Qualitative identification of Cu, Sn, Pb, Ni, and Fe in Cu-alloys is presented. The method involves anodic sampling of alloys, separation and identification by thin-layer chromatography (TLC). The powerful desktop-computer tool makes it easy to optimize ternary solvent mixtures. Optimization was performed graphically by means of Rsi≥1 as a selected separation criterion. Mobile phase composition for optimal separation was determined as MeOH−HCl−H2O (60:35:5, v/v). The method was applied to Persian helmet as real sample.

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Cover JPC - Journal of Planar Chromatography - Modern TLC
JPC - Journal of Planar Chromatography - Modern TLC
Print ISSN:
0933-4173
Online ISSN:
1789-0993

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Manuscript Submission: HERE

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Journal of Planar Chromatography - Modern TLC
Language English
Size A4
Year of
Foundation		 1988
Volumes
per Year		 1
Issues
per Year		 6
Founder Akadémiai Kiadó
Founder's
Address		 H-1117 Budapest, Hungary 1516 Budapest, PO Box 245.
Publisher Akadémiai Kiadó
Springer Nature Switzerland AG
Publisher's
Address		 H-1117 Budapest, Hungary 1516 Budapest, PO Box 245.
CH-6330 Cham, Switzerland Gewerbestrasse 11.
Responsible
Publisher		 Chief Executive Officer, Akadémiai Kiadó
ISSN 0933-4173 (Print)
ISSN 1789-0993 (Online)

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